11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide

Base Information

Chemical Name:11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide
CAS No.:119327-28-5
Molecular Formula:C₁₈H₁₃OPS₂
Molecular Weight:340.406
Hs Code.:

11-Phenyl-11H-dibenzo<c,f><1,2,5>dithiaphosphepin-11-oxide

Synonyms:11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide

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Chemical Property of 11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide

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Technology Process of 11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide

There total 3 articles about 11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 119327-21-8
C₁₈H₁₅OPS₂

: 119327-28-5
11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide

Guidance literature:: With dimethyl sulfoxide; at 90 ℃; for 24h;
DOI:10.1021/ja00188a071

Reference yield:

: 824-72-6
P,P-dichlorophenylphosphine oxide

: 119327-28-5
11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, TMEDA / 1.) hexane, 2.) THF, -78 deg C to room temp., overnight

2: 93 percent / DMSO / 24 h / 90 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dimethyl sulfoxide;
DOI:10.1021/ja00188a071

Reference yield:

: 108-98-5
thiophenol

: 119327-28-5
11-Phenyl-11H-dibenzo<1,2,5>dithiaphosphepin-11-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi, TMEDA / 1.) hexane, 2.) THF, -78 deg C to room temp., overnight

2: 93 percent / DMSO / 24 h / 90 °C

With n-butyllithium; N,N,N,N,-tetramethylethylenediamine; dimethyl sulfoxide;
DOI:10.1021/ja00188a071