N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine

Base Information

• Chemical Name: N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine
• CAS No.: 1019849-43-4
• Molecular Formula: C₇₀H₇₄N₄O₁₅
• Molecular Weight: 1211.38

Synonyms:N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine

Chemical Property of N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine

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Technology Process of N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine

There total 1 articles about N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

Nα-(9-fluorenylmethoxycarbonyl)-Nγ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine tert-butyl ester (1093115-84-4) → Nα-(9-fluorenylmethoxycarbonyl)-Nγ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine (1019849-43-4)

Guidance literature:

With triethylsilane; trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2.5h;

DOI:10.1016/j.carres.2008.08.024

Reference yield:

Nα-(9-fluorenylmethoxycarbonyl)-Nγ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine (1019849-43-4) + C100H138ClN10O19Pol → C170H210ClN14O33Pol

Guidance literature:

N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine; With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In 1-methyl-pyrrolidin-2-one; at 20 ℃; for 1h;

C₁₀₀H₁₃₈ClN₁₀O₁₉Pol; In 1-methyl-pyrrolidin-2-one; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.carres.2008.08.024

upstream raw materials:

N^α-(9-fluorenylmethoxycarbonyl)-N^γ-[(2-acetamido-3,4,6-tri-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-2-acetamido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl]-L-asparagine tert-butyl ester

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