8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

Base Information

Chemical Name:8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine
CAS No.:1612843-14-7
Molecular Formula:C₄₁H₃₈N₄O₄
Molecular Weight:650.777
Hs Code.:

Synonyms:8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

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Chemical Property of 8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

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Technology Process of 8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

There total 4 articles about 8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: 1612843-09-0
8,11-dibromo-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

: 13331-27-6
m-nitrobenzene boronic acid

: 1612843-14-7
8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

: 1612843-15-8
11-(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

Guidance literature:: With potassium phosphate; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In 1,4-dioxane; water; at 90 ℃; for 6h; Inert atmosphere;
DOI:10.1021/ol501226x

Reference yield:

: 1445988-71-5
bis[2-(2-octyn-1-yl)phenyl]carbodiimide

: 1612843-14-7
8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: Rh(dppp)2Cl / toluene / 0.33 h / 120 °C

1.2: 12 h / 20 °C

2.1: N-Bromosuccinimide / acetonitrile / 20 °C

3.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,4-dioxane / Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Rh(dppp)2Cl; potassium carbonate; In 1,4-dioxane; water; toluene; acetonitrile; 3.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/acs.joc.7b02674

Reference yield:

: 1220997-85-2
1-azido-2-(oct-2-ynyl)benzene

: 1612843-14-7
8,11-bis(3-nitrophenyl)-6,7-dipentylbenzo[g]indolo[1,2-a][1,8]naphthyridine

Guidance literature:: Multi-step reaction with 5 steps

1.1: dichloromethane / 20 °C

2.1: dichloromethane / 20 °C

3.1: Rh(dppp)2Cl / toluene / 0.33 h / 120 °C

3.2: 12 h / 20 °C

4.1: N-Bromosuccinimide / acetonitrile / 20 °C

5.1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,4-dioxane / Reflux

With N-Bromosuccinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; Rh(dppp)2Cl; potassium carbonate; In 1,4-dioxane; dichloromethane; water; toluene; acetonitrile; 2.1: |Aza-Wittig Reaction / 5.1: |Suzuki-Miyaura Coupling;
DOI:10.1021/acs.joc.7b02674