1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine

Base Information

Chemical Name:1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine
CAS No.:849334-33-4
Molecular Formula:C₁₉H₂₉NO₄S
Molecular Weight:367.51
Hs Code.:

Synonyms:1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine

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Chemical Property of 1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine

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Technology Process of 1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine

There total 6 articles about 1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 31.0%

: 849334-36-7
1-(5,5-dimethoxypentyl)-3-(4-methylphenylsulfonyl)-2,6-azinanedione

: 849334-33-4
1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine

Guidance literature:: 1-(5,5-dimethoxypentyl)-3-(4-methylphenylsulfonyl)-2,6-azinanedione; With N-Bromosuccinimide; sodium hydrogencarbonate; In acetonitrile; at 20 ℃; for 1.5h;

With lithium aluminium tetrahydride; In tetrahydrofuran; for 2h; Heating;
DOI:10.3987/COM-04-10274

Reference yield:

: 849334-35-6
1-(5-hydroxypentyl)-2-(4-methylphenylsulfonyl)acetamide

: 849334-33-4
1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine

Guidance literature:: Multi-step reaction with 4 steps

1.1: 62 percent / sodium hydride / tetrahydrofuran / 10 h / 20 °C

2.1: 73 percent / pyridinium chlorochromate; Celite / CH₂Cl₂ / 18 h / 20 °C

3.1: 99 percent / p-toluenesulfonic acid / methanol / 2 h / 20 °C

4.1: N-bromosuccinimide; sodium bicarbonate / acetonitrile / 1.5 h / 20 °C

4.2: 31 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / Heating

With N-Bromosuccinimide; Celite; sodium hydride; sodium hydrogencarbonate; toluene-4-sulfonic acid; pyridinium chlorochromate; In tetrahydrofuran; methanol; dichloromethane; acetonitrile;
DOI:10.3987/COM-04-10274

Reference yield:

: 849334-39-0
5-[2,6-dioxo-3-(toluene-4-sulfonyl)-piperidin-1-yl]-pentanal

: 849334-33-4
1-(5,5-dimethoxypentyl)-5-(4-methylphenylsulfonyl)-1,2,3,4-tetrahydropyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 99 percent / p-toluenesulfonic acid / methanol / 2 h / 20 °C

2.1: N-bromosuccinimide; sodium bicarbonate / acetonitrile / 1.5 h / 20 °C

2.2: 31 percent / lithium aluminum hydride / tetrahydrofuran / 2 h / Heating

With N-Bromosuccinimide; sodium hydrogencarbonate; toluene-4-sulfonic acid; In methanol; acetonitrile;
DOI:10.3987/COM-04-10274