N₁-benzyloxycarbonyl-N₂-(tert-butoxycarbonyl)-N₃-trifluoromethanesulfonylguanidine

Base Information

• Chemical Name: N₁-benzyloxycarbonyl-N₂-(tert-butoxycarbonyl)-N₃-trifluoromethanesulfonylguanidine
• CAS No.: 216584-27-9
• Molecular Formula: C₁₅H₁₈F₃N₃O₆S
• Molecular Weight: 425.386

Synonyms:N₁-benzyloxycarbonyl-N₂-(tert-butoxycarbonyl)-N₃-trifluoromethanesulfonylguanidine

Chemical Property of N₁-benzyloxycarbonyl-N₂-(tert-butoxycarbonyl)-N₃-trifluoromethanesulfonylguanidine

Chemical Property:

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Technology Process of N₁-benzyloxycarbonyl-N₂-(tert-butoxycarbonyl)-N₃-trifluoromethanesulfonylguanidine

There total 1 articles about N₁-benzyloxycarbonyl-N₂-(tert-butoxycarbonyl)-N₃-trifluoromethanesulfonylguanidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

trifluoromethylsulfonic anhydride (358-23-6) + N1-(benzyloxycarbonyl)-N2-(tert-butoxycarbonyl)guanidine (194985-14-3) → N1-benzyloxycarbonyl-N2-(tert-butoxycarbonyl)-N3-trifluoromethanesulfonylguanidine (216584-27-9)

Guidance literature:

N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)guanidine; With sodium hydride; In chlorobenzene; mineral oil; at 0 ℃; for 1h; Inert atmosphere;

trifluoromethylsulfonic anhydride; In chlorobenzene; mineral oil; at -45 - 20 ℃; Inert atmosphere;

DOI:10.1021/jm9000693

Reference yield: 88.0%

N1-benzyloxycarbonyl-N2-(tert-butoxycarbonyl)-N3-trifluoromethanesulfonylguanidine (216584-27-9) + 4-(3-aminopropyl)-1-(triphenylmethyl)-imidazole (195053-89-5) → N1-(benzyloxycarbonyl)-N2-(tert-butoxycarbonyl)-N3-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine (1146622-74-3)

Guidance literature:

With triethylamine; In dichloromethane; at 20 ℃;

DOI:10.1021/jm9000693

upstream raw materials:

trifluoromethylsulfonic anhydride

N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)guanidine

Downstream raw materials:

N₁-(benzyloxycarbonyl)-N₂-(tert-butoxycarbonyl)-N₃-[3-(1-trityl-1H-imidazol-4-yl)propyl]-guanidine

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