C₅₄H₆₈N₄O₈S₂

Base Information

Chemical Name:C₅₄H₆₈N₄O₈S₂
CAS No.:1449429-36-0
Molecular Formula:C₅₄H₆₈N₄O₈S₂
Molecular Weight:965.288
Hs Code.:

C<sub>54</sub>H<sub>68</sub>N<sub>4</sub>O<sub>8</sub>S<sub>2</sub>

Synonyms:C₅₄H₆₈N₄O₈S₂

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Chemical Property of C₅₄H₆₈N₄O₈S₂

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Technology Process of C₅₄H₆₈N₄O₈S₂

There total 8 articles about C₅₄H₆₈N₄O₈S₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1449429-35-9
C₆₄H₈₄N₄O₁₂S₂

: 1449429-36-0
C₅₄H₆₈N₄O₈S₂

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;
DOI:10.1002/chem.201204556

Reference yield:

: 1449429-31-5
C₂₀H₁₆S₂

: 1449429-36-0
C₅₄H₆₈N₄O₈S₂

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide; oxygen / N,N-dimethyl-formamide / 120 h / 70 °C

2: thionyl chloride; N,N-dimethyl-formamide / 6 h / 60 °C / Inert atmosphere

3: pyridine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

4: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With pyridine; thionyl chloride; oxygen; N,N-dimethyl-formamide; trifluoroacetic acid; potassium hydroxide; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/chem.201204556

Reference yield:

: C₂₂H₁₆O₄

: 1449429-36-0
C₅₄H₆₈N₄O₈S₂

Guidance literature:: Multi-step reaction with 8 steps

1: potassium carbonate / methanol / 2 h / 0 - 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 3 h / -100 - 0 °C / Inert atmosphere

3: 1,1'-bis-(diphenylphosphino)ferrocene; sodium t-butanolate; palladium diacetate / toluene / 1 h / 100 °C / Inert atmosphere

4: tetrabutyl ammonium fluoride; acetic acid / tetrahydrofuran / 0.33 h / 0 °C / Inert atmosphere

5: potassium hydroxide; oxygen / N,N-dimethyl-formamide / 120 h / 70 °C

6: thionyl chloride; N,N-dimethyl-formamide / 6 h / 60 °C / Inert atmosphere

7: pyridine / dichloromethane / 18 h / 0 - 20 °C / Inert atmosphere

8: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C / Inert atmosphere

With pyridine; 1,1'-bis-(diphenylphosphino)ferrocene; thionyl chloride; tetrabutyl ammonium fluoride; oxygen; palladium diacetate; potassium carbonate; acetic acid; triethylamine; N,N-dimethyl-formamide; trifluoroacetic acid; potassium hydroxide; sodium t-butanolate; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; toluene;
DOI:10.1002/chem.201204556