3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane

Base Information

Chemical Name:3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane
CAS No.:172024-30-5
Molecular Formula:C₂₂H₃₈O₅Si
Molecular Weight:410.626
Hs Code.:

Synonyms:3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane

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Technology Process of 3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane

There total 2 articles about 3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: tert-Butyl-[3-((E)-2-ethoxymethyl-1-methoxy-3,3-dimethyl-but-1-enyl)-phenoxy]-dimethyl-silane

: 172024-30-5
3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane

Guidance literature:: With oxygen; 5,15,10,20-tetraphenylporphyrin; In dichloromethane; at 0 ℃; for 3h; Irradiation;
DOI:10.1016/0040-4039(96)01282-8

Reference yield:

: 172024-30-5
3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane

Guidance literature:

Reference yield:

: 172024-30-5
3-t-butyl-4-[3-(t-butyldimethylsiloxy)phenyl]-3-ethoxymethyl-4-methoxy-1,2-dioxetane

: methyl m-oxybenzoate ion

: 1-ethoxy-3,3-dimethylbutan-2-one

Guidance literature:: With tetrabutyl ammonium fluoride; In dimethyl sulfoxide; at 25 ℃; Quantum yield; substrate half-life < 1 s; chemiluminescence: λ(max)= 463 nm;
DOI:10.1016/0040-4039(96)01282-8