C₃₀H₄₀O₅Si

Base Information

Chemical Name:C₃₀H₄₀O₅Si
CAS No.:1265215-34-6
Molecular Formula:C₃₀H₄₀O₅Si
Molecular Weight:508.73
Hs Code.:

C<sub>30</sub>H<sub>40</sub>O<sub>5</sub>Si

Synonyms:C₃₀H₄₀O₅Si

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Chemical Property of C₃₀H₄₀O₅Si

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Technology Process of C₃₀H₄₀O₅Si

There total 17 articles about C₃₀H₄₀O₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1265215-07-3
C₃₆H₅₄O₅Si₂

: 1265215-34-6
C₃₀H₄₀O₅Si

Guidance literature:: With water; acetic acid; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1021/ol103024z

Reference yield:

: 1033282-40-4
diethyl 4-ethylideneheptanedioate

: 1265215-34-6
C₃₀H₄₀O₅Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C

2.1: 1H-imidazole / dichloromethane / 2 h / 0 °C

3.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.33 h / -78 °C

3.2: 0.5 h / -78 °C

4.1: potassium hexamethylsilazane / 1,2-dimethoxyethane / -78 °C

5.1: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / methanol / 1 h / Inert atmosphere; Reflux

6.1: potassium trimethylsilonate / tetrahydrofuran; diethyl ether / 13 h / 45 °C

7.1: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

8.1: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 0 °C

9.1: dmap; triethylamine / dichloromethane / 4 h / 20 °C

10.1: tetrahydrofuran / 12 h / -40 °C

11.1: lithium diisopropyl amide / tetrahydrofuran / 0.33 h / -78 °C

12.1: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h

13.1: methanol; potassium carbonate / 0.33 h / 20 °C

14.1: tetrahydrofuran; diethyl ether / 0.33 h / -78 °C

15.1: dmap; triethylamine / dichloromethane / 10 h / 20 °C

16.1: water; acetic acid / tetrahydrofuran / 1 h / 0 °C

With 1H-imidazole; methanol; dmap; lithium aluminium tetrahydride; oxalyl dichloride; potassium trimethylsilonate; water; palladium diacetate; potassium hexamethylsilazane; potassium carbonate; acetic acid; dimethyl sulfoxide; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; tris-(o-tolyl)phosphine; lithium diisopropyl amide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; 3.1: Swern oxidation / 3.2: Swern oxidation / 4.1: Horner-Wadsworth-Emmons olefination / 5.1: Mizoroki-Heck cyclization / 12.1: Rubottom oxidation;
DOI:10.1021/ol103024z

Reference yield:

: 1265214-87-6
C₂₅H₃₄O₂Si

: 1265215-34-6
C₃₀H₄₀O₅Si

Guidance literature:: Multi-step reaction with 13 steps

1: potassium hexamethylsilazane / 1,2-dimethoxyethane / -78 °C

2: palladium diacetate; triethylamine; tris-(o-tolyl)phosphine / methanol / 1 h / Inert atmosphere; Reflux

3: potassium trimethylsilonate / tetrahydrofuran; diethyl ether / 13 h / 45 °C

4: dmap; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 8 h / 0 °C

5: 9-bora-bicyclo[3.3.1]nonane / tetrahydrofuran / 4 h / 0 °C

6: dmap; triethylamine / dichloromethane / 4 h / 20 °C

7: tetrahydrofuran / 12 h / -40 °C

8: lithium diisopropyl amide / tetrahydrofuran / 0.33 h / -78 °C

9: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 0.33 h

10: methanol; potassium carbonate / 0.33 h / 20 °C

11: tetrahydrofuran; diethyl ether / 0.33 h / -78 °C

12: dmap; triethylamine / dichloromethane / 10 h / 20 °C

13: water; acetic acid / tetrahydrofuran / 1 h / 0 °C

With methanol; dmap; potassium trimethylsilonate; water; palladium diacetate; potassium hexamethylsilazane; potassium carbonate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; 9-bora-bicyclo[3.3.1]nonane; 3-chloro-benzenecarboperoxoic acid; tris-(o-tolyl)phosphine; lithium diisopropyl amide; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; diethyl ether; dichloromethane; 1: Horner-Wadsworth-Emmons olefination / 2: Mizoroki-Heck cyclization / 9: Rubottom oxidation;
DOI:10.1021/ol103024z