2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone

Base Information

Chemical Name:2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone
CAS No.:1335227-33-2
Molecular Formula:C₁₅H₁₁ClN₄O₂S₂
Molecular Weight:378.863
Hs Code.:

Synonyms:2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone

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Chemical Property of 2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone

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Technology Process of 2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone

There total 3 articles about 2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 41011-01-2
2-bromo-1-(3-chloro-phenyl)-ethanone

: 1024561-99-6
C₇H₆N₄OS₂

: 1335227-33-2
2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone

Guidance literature:: In acetone; at 20 ℃; for 8h;
DOI:10.3390/molecules16097662

Reference yield:

: 60458-70-0
2-[((pyrimidin-2-yl)thio)]acetohydrazide

: 1335227-33-2
2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium hydroxide / ethanol / 10 h / Reflux

1.2: pH 5 - 6

2.1: acetone / 8 h / 20 °C

With potassium hydroxide; In ethanol; acetone;
DOI:10.3390/molecules16097662

Reference yield:

: 60458-72-2
ethyl α-[(2-pyrimidyl)thio]acetate

: 1335227-33-2
2-[5-[(pyrimidin-2-ylthio)methyl]-1,3,4-oxadiazol-2-ylthio]-3'-chloroacetophenone

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrazine hydrate / ethanol / 3 h / 20 °C

2.1: potassium hydroxide / ethanol / 10 h / Reflux

2.2: pH 5 - 6

3.1: acetone / 8 h / 20 °C

With hydrazine hydrate; potassium hydroxide; In ethanol; acetone;
DOI:10.3390/molecules16097662