Technology Process of C18H13ClN2O3
There total 6 articles about C18H13ClN2O3 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
oxalyl dichloride;
N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1,2-dichloro-benzene / 4 h / 100 °C
2: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 - 3 h / 120 - 140 °C / Microwave irradiation
3: cyclohexa-1,4-diene / palladium 10% on activated carbon / tetrahydrofuran / 0.17 - 0.25 h / 20 - 90 °C / Microwave irradiation
4: lithium hydroxide / tetrahydrofuran / 2 h
5: oxalyl dichloride / N,N-dimethyl-formamide
With
lithium hydroxide; oxalyl dichloride; cyclohexa-1,4-diene; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon; N,N-dimethyl-formamide;
In
tetrahydrofuran; 1,2-dichloro-benzene;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 1 - 3 h / 120 - 140 °C / Microwave irradiation
2: cyclohexa-1,4-diene / palladium 10% on activated carbon / tetrahydrofuran / 0.17 - 0.25 h / 20 - 90 °C / Microwave irradiation
3: lithium hydroxide / tetrahydrofuran / 2 h
4: oxalyl dichloride / N,N-dimethyl-formamide
With
lithium hydroxide; oxalyl dichloride; cyclohexa-1,4-diene; N-ethyl-N,N-diisopropylamine;
palladium 10% on activated carbon; N,N-dimethyl-formamide;
In
tetrahydrofuran;