[1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol

Base Information

• Chemical Name: [1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol
• CAS No.: 863097-82-9
• Molecular Formula: C₂₀H₁₆Cl₃NO
• Molecular Weight: 392.712

Synonyms:[1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol

Chemical Property of [1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol

Chemical Property:

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Technology Process of [1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol

There total 2 articles about [1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanone (863097-46-5) → [1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol (863097-82-9)

Guidance literature:

With lithium aluminium tetrahydride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1021/jm048997u

Reference yield:

[4-(4-Chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanone (170939-26-1) → [1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol (863097-82-9)

Guidance literature:

Multi-step reaction with 2 steps

1: 84 percent / K₂CO₃ / dimethylformamide / 20 h / 90 °C

2: LiAlH₄ / tetrahydrofuran / 2 h / 20 °C

With lithium aluminium tetrahydride; potassium carbonate; In tetrahydrofuran; N,N-dimethyl-formamide;

DOI:10.1021/jm048997u

Reference yield:

[1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanol (863097-82-9) + 1,1'-carbonyldiimidazole (530-62-1) → 1-[[1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methyl]-1H-imidazole

Guidance literature:

In acetonitrile; at 20 ℃; for 1h;

DOI:10.1021/jm048997u

upstream raw materials:

[1-allyl-4-(4-chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanone

[4-(4-Chloro-phenyl)-1H-pyrrol-3-yl]-(2,4-dichloro-phenyl)-methanone

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