C₇₀H₁₂₃O₁₆Si₂N

Base Information

Chemical Name:C₇₀H₁₂₃O₁₆Si₂N
CAS No.:930803-69-3
Molecular Formula:C₇₀H₁₂₃NO₁₆Si₂
Molecular Weight:1290.91
Hs Code.:

C<sub>70</sub>H<sub>123</sub>O<sub>16</sub>Si<sub>2</sub>N

Synonyms:C₇₀H₁₂₃O₁₆Si₂N

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Chemical Property of C₇₀H₁₂₃O₁₆Si₂N

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Technology Process of C₇₀H₁₂₃O₁₆Si₂N

There total 50 articles about C₇₀H₁₂₃O₁₆Si₂N which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 930803-47-7
C₇₀H₁₂₁O₁₅Si₂N

: 930803-69-3
C₇₀H₁₂₃O₁₆Si₂N

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; water; at 0 ℃;
DOI:10.1002/anie.200604053

Reference yield: 89.0%

: C₇₀H₁₂₁NO₁₅Si₂

: 930803-69-3
C₇₀H₁₂₃O₁₆Si₂N

Guidance literature:: With lithium hydroxide; water; In tetrahydrofuran; at 0 ℃; for 1h;
DOI:10.1002/chem.200801656

Reference yield:

: 930803-25-1
C₁₀H₁₅S₂O₂Br

: 930803-69-3
C₇₀H₁₂₃O₁₆Si₂N

Guidance literature:: Multi-step reaction with 15 steps

1.1: 99 percent / diisobutylaluminum hydride / CH₂Cl₂ / -45 °C

2.1: 70 percent / methanesulfonyl chloride; triethylamine; 4-(dimethylamino)pyridine / lithium bromide / CH₂Cl₂; dimethylformamide

3.1: 99 percent / LiBHEt₃ / tetrahydrofuran / 0 °C

4.1: tert-butyllithium / tetrahydrofuran / -96 - -78 °C

5.1: 99 percent / 2,6-lutidine / CH₂Cl₂ / 0.67 h / -78 °C

6.1: 77 percent / tert-butyllithium; hexamethylphosphoramide / tetrahydrofuran / -78 - -40 °C

7.1: 84 percent / (bis(trifluoroacetoxy)iodo)benzene / tetrahydrofuran; H₂O; methanol / 20 °C

8.1: 84 percent / 1,3-dicyclohexylcarbodiimide; 4-(dimethylamino)pyridine / CH₂Cl₂ / 24 h / -5 °C

9.1: 93 percent / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone / CH₂Cl₂ / 20 °C / pH 7

10.1: 99 percent / (COCl)2; dimethyl sulfoxide; triethylamine / CH₂Cl₂

11.1: 82 percent / CrCl₂ / tetrahydrofuran / 0 - 20 °C

12.1: N-methylpyrrolidinone; [Pd{P(2-furyl)3}2Cl₂]; hexamethyltin / 20 °C

12.2: [Pd{P(2-furyl)3}2Cl₂]; N-methylpyrrolidinone / 20 °C

13.1: 81 percent / LiAlH(OtBu)3 / tetrahydrofuran / -10 °C

14.1: 81 percent / 4-pyrrolidinopyridine / CH₂Cl₂

15.1: 89 percent / lithium hydroxide / H₂O; tetrahydrofuran / 0 °C

With 2,6-dimethylpyridine; 1-methyl-pyrrolidin-2-one; chromium dichloride; N,N,N,N,N,N-hexamethylphosphoric triamide; dmap; lithium hydroxide; oxalyl dichloride; tert.-butyl lithium; hexamethyldistannane; diisobutylaluminium hydride; lithium triethylborohydride; 4-pyrrolidin-1-ylpyridine; dimethyl sulfoxide; methanesulfonyl chloride; lithium tri-t-butoxyaluminum hydride; triethylamine; dicyclohexyl-carbodiimide; 2,3-dicyano-5,6-dichloro-p-benzoquinone; bis-[(trifluoroacetoxy)iodo]benzene; lithium bromide; In tetrahydrofuran; methanol; dichloromethane; water; N,N-dimethyl-formamide; 10.1: Swern oxidation;
DOI:10.1002/anie.200604053