1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane

Base Information

Chemical Name:1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane
CAS No.:102563-50-8
Molecular Formula:C₂₇H₂₇O₆P
Molecular Weight:478.482
Hs Code.:

Synonyms:1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane

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Technology Process of 1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane

There total 2 articles about 1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 186581-53-3,908094-01-9,334-88-3
diazomethane

: 102563-59-7
C₂₆H₂₅O₆P

: 102563-50-8
1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane

Guidance literature:: In tetrahydrofuran; diethyl ether; dichloromethane; at 20 ℃;
DOI:10.1055/s-1985-31339

Reference yield:

: 1099-45-2
ethyl (triphenylphosphoranylidene)acetate

: 102563-50-8
1-Ethoxycarbonyl-3-(methoxycarbonylmethoxy)-2-oxopropylidenetriphenylphosphorane

Guidance literature:: Multi-step reaction with 2 steps

1: 91 percent / CHCl₃ / 1 h / Ambient temperature

2: 85 percent / CH₂Cl₂; tetrahydrofuran; diethyl ether / 20 °C

In tetrahydrofuran; diethyl ether; dichloromethane; chloroform;
DOI:10.1055/s-1985-31339