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C24H26ClNO5

Base Information
  • Chemical Name:C24H26ClNO5
  • CAS No.:1613154-18-9
  • Molecular Formula:C24H26ClNO5
  • Molecular Weight:443.927
  • Hs Code.:
C<sub>24</sub>H<sub>26</sub>ClNO<sub>5</sub>

Synonyms:C24H26ClNO5

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Chemical Property of C24H26ClNO5
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Technology Process of C24H26ClNO5

There total 7 articles about C24H26ClNO5 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; for 2h; Reflux;
DOI:10.1039/c4ob00842a
Guidance literature:
Multi-step reaction with 6 steps
1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 20 °C
2: sodium hydroxide / ethanol / 3 h / Reflux
3: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / Reflux
4: N-Bromosuccinimide; dmap / tetrahydrofuran; methanol / 1 h / 0 °C
5: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C
6: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Reflux
With dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene; 3: |Curtius Rearrangement;
DOI:10.1039/c4ob00842a
Guidance literature:
Multi-step reaction with 5 steps
1: sodium hydroxide / ethanol / 3 h / Reflux
2: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / Reflux
3: N-Bromosuccinimide; dmap / tetrahydrofuran; methanol / 1 h / 0 °C
4: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C
5: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Reflux
With dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene; 2: |Curtius Rearrangement;
DOI:10.1039/c4ob00842a
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