Technology Process of C24H26ClNO5
There total 7 articles about C24H26ClNO5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride;
In
toluene;
for 2h;
Reflux;
DOI:10.1039/c4ob00842a
- Guidance literature:
-
Multi-step reaction with 6 steps
1: tetra-(n-butyl)ammonium iodide; potassium carbonate / N,N-dimethyl-formamide / 20 °C
2: sodium hydroxide / ethanol / 3 h / Reflux
3: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / Reflux
4: N-Bromosuccinimide; dmap / tetrahydrofuran; methanol / 1 h / 0 °C
5: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C
6: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Reflux
With
dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; potassium carbonate; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene;
3: |Curtius Rearrangement;
DOI:10.1039/c4ob00842a
- Guidance literature:
-
Multi-step reaction with 5 steps
1: sodium hydroxide / ethanol / 3 h / Reflux
2: diphenyl phosphoryl azide; N-ethyl-N,N-diisopropylamine / Reflux
3: N-Bromosuccinimide; dmap / tetrahydrofuran; methanol / 1 h / 0 °C
4: sodium hydride; tetra-(n-butyl)ammonium iodide / N,N-dimethyl-formamide / 20 °C
5: 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride / toluene / 2 h / Reflux
With
dmap; N-Bromosuccinimide; 2,2'-azobis(isobutyronitrile); diphenyl phosphoryl azide; tri-n-butyl-tin hydride; tetra-(n-butyl)ammonium iodide; sodium hydride; N-ethyl-N,N-diisopropylamine; sodium hydroxide;
In
tetrahydrofuran; methanol; ethanol; N,N-dimethyl-formamide; toluene;
2: |Curtius Rearrangement;
DOI:10.1039/c4ob00842a