2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

Base Information

Chemical Name:2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine
CAS No.:78796-89-1
Molecular Formula:C₃₃H₂₆N₄O₉
Molecular Weight:622.591
Hs Code.:

Synonyms:2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

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Chemical Property of 2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

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Technology Process of 2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

There total 4 articles about 2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 6343-98-2
2-hydrazino-5-nitropyridine

: 78810-53-4
benzyl (2,3,4-tri-O-benzoyl-6-deoxy-L-manno-hexopyranosyl)thioimidate hydrochloride

: 78796-89-1
2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

Guidance literature:: With pyridine; In dichloromethane; for 120h; Heating;
DOI:10.1021/jm00143a006

Reference yield:

: 61198-83-2,73891-00-6,73891-01-7,113567-33-2,113567-34-3,122089-70-7,135266-93-2,135266-94-3,140223-15-0,141115-69-7,148152-57-2,71155-57-2
1,2,3,4-tetra-O-benzoyl-α/β-L-rhamnopyranose

: 78796-89-1
2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

Guidance literature:: Multi-step reaction with 4 steps

1: 77 percent / hydrobromic acid / acetic acid / 4 °C

2: 14 percent / nitromethane / 72 h

3: 82 percent / hydrochloric acid / diethyl ether / 4 °C

4: 35 percent / pyridine / CH₂Cl₂ / 120 h / Heating

With pyridine; hydrogenchloride; hydrogen bromide; In diethyl ether; nitromethane; dichloromethane; acetic acid;
DOI:10.1021/jm00143a006

Reference yield:

: 14218-08-7,41881-44-1,53297-33-9,60820-93-1,61198-82-1,67986-91-8,73068-86-7,131897-72-8,131897-73-9
2,3,4-tri-O-benzoyl-α-L-rhamnopyranosyl bromide

: 78796-89-1
2-(2',3',4'-tri-O-benzoyl-6'-deoxy-α-L-manno-hexopyranosyl)-6-nitro<1,2,4>triazolo<1,5-a>pyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 14 percent / nitromethane / 72 h

2: 82 percent / hydrochloric acid / diethyl ether / 4 °C

3: 35 percent / pyridine / CH₂Cl₂ / 120 h / Heating

With pyridine; hydrogenchloride; In diethyl ether; nitromethane; dichloromethane;
DOI:10.1021/jm00143a006