Technology Process of C29H52N2O7Si
There total 4 articles about C29H52N2O7Si which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
triphenylphosphine; diethylazodicarboxylate;
In
dichloromethane;
Ambient temperature;
DOI:10.1016/0040-4039(92)88182-5
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 86 percent / 4A molecular sieves / toluene / 2 h / 70 °C
2: 97 percent / H2 / PtO2 / ethanol / 120 h / Ambient temperature
3: 91 percent / Ca(BH4)2 / ethanol; tetrahydrofuran / -20 deg C to r.t.
4: 92 percent / Ph3P, DEAD / CH2Cl2 / Ambient temperature
With
calcium borohydride; 4 A molecular sieve; hydrogen; triphenylphosphine; diethylazodicarboxylate;
platinum(IV) oxide;
In
tetrahydrofuran; ethanol; dichloromethane; toluene;
DOI:10.1016/0040-4039(92)88182-5
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 97 percent / H2 / PtO2 / ethanol / 120 h / Ambient temperature
2: 91 percent / Ca(BH4)2 / ethanol; tetrahydrofuran / -20 deg C to r.t.
3: 92 percent / Ph3P, DEAD / CH2Cl2 / Ambient temperature
With
calcium borohydride; hydrogen; triphenylphosphine; diethylazodicarboxylate;
platinum(IV) oxide;
In
tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1016/0040-4039(92)88182-5