(R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion

Base Information

Chemical Name:(R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion
CAS No.:1372400-65-1
Molecular Formula:C₂₆H₂₄O₅
Molecular Weight:416.474
Hs Code.:

Synonyms:(R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion

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Chemical Property of (R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion

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Technology Process of (R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion

There total 3 articles about (R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1352708-09-8
trimethyl((5-methyl-2-phenyl-1,3,2-dioxaborinan-5-yl)methoxy)silane

: 666698-12-0
C₂₀H₁₈O₅

: 1372400-65-1
(R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion

Guidance literature:: With chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide; In 1,4-dioxane; at 20 ℃;
DOI:10.1039/c1ob06586f

Reference yield:

: 52205-01-3
(5-methyl-2-phenyl-[1,3,2]dioxaborinan-5-yl)-methanol

: 1372400-65-1
(R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

2: chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide / 1,4-dioxane / 20 °C

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triethylamine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane;
DOI:10.1039/c1ob06586f

Reference yield:

: 98-80-6
phenylboronic acid

: 1372400-65-1
(R)-5-((2-(benzyloxy)phenyl)(phenyl)methyl)-2,2-dimethyl-1,3-dioxane-4,6-dion

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 3 h

2: triethylamine / tetrahydrofuran / 24 h / 0 - 20 °C / Inert atmosphere

3: chloro(1,5-cyclooctadiene)rhodium(I) dimer; potassium hydroxide / 1,4-dioxane / 20 °C

With chloro(1,5-cyclooctadiene)rhodium(I) dimer; triethylamine; potassium hydroxide; In tetrahydrofuran; 1,4-dioxane; toluene;
DOI:10.1039/c1ob06586f