8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene

Base Information

Chemical Name:8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene
CAS No.:1449105-45-6
Molecular Formula:C₂₂H₂₂BF₂N₃O
Molecular Weight:393.244
Hs Code.:

Synonyms:8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene

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Technology Process of 8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene

There total 2 articles about 8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1449105-34-3
4,4-difluoro-1,3,5,8-tetramethyl-4-bora-3a,4a-diaza-s-indacene

: 122-85-0
para-acetamidobenzaldehyde

: 1449105-45-6
8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: With piperidine; acetic acid; In benzene; for 5h; Inert atmosphere; Reflux;
DOI:10.1021/ol401993p

Reference yield:

: 636-41-9
2-methyl-1H-pyrrole

: 1500-93-2
1-(3,5-dimethyl-1H-pyrrol-2-yl)ethan-1-one

: 1449105-45-6
8-(4-acetamidostyryl)-4,4-difluoro-1,3,5-trimethyl-4-bora-3a,4a-diaza-s-indacene

Guidance literature:: Multi-step reaction with 2 steps

1.1: trichlorophosphate / dichloromethane / 1 h / 20 °C / Inert atmosphere

1.2: 12 h / 20 °C / Inert atmosphere

1.3: 0.5 h / 20 °C / Inert atmosphere

2.1: piperidine; acetic acid / benzene / 5 h / Inert atmosphere; Reflux

With piperidine; acetic acid; trichlorophosphate; In dichloromethane; benzene; 2.1: |Knoevenagel Condensation;
DOI:10.1021/ol401993p