2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester

Base Information

Chemical Name:2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester
CAS No.:1246197-96-5
Molecular Formula:C₂₅H₃₅N₃O₄S
Molecular Weight:473.637
Hs Code.:

Synonyms:2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester

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Chemical Property of 2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester

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Technology Process of 2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester

There total 1 articles about 2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 1246198-68-4
2-chloro-6-[methyl-(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester

: 116373-23-0
N-benzyl-N-(cyclopropylmethyl)amine

: 1246197-96-5
2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester

Guidance literature:: With potassium phosphate; dimethyl amine; bis(tri-tert-butylphosphine)palladium⁽⁰⁾; at 130 ℃; for 1.5h; microwave irradiation; Inert atmosphere;

Reference yield:

: 1246197-96-5
2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester

: 76-05-1
trifluoroacetic acid

: 2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid trifluoroacetate

Guidance literature:: 2-(benzyl-cyclopropylmethyl-amino)-6-[methyl(propane-2-sulfonyl)amino]isonicotinic acid tert-butyl ester; With hydrogen; palladium(II) hydroxide; In methanol; ethyl acetate; at 60 ℃; under 15001.5 Torr;

trifluoroacetic acid; In dichloromethane; for 1h;