Technology Process of C27H38O5
There total 5 articles about C27H38O5 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; sodium hydride;
In
N,N-dimethyl-formamide;
at 20 ℃;
DOI:10.1002/anie.200604053
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium carbonate / methanol / 20 °C
2: 99 percent / sodium hydride; tetrabutylammonium iodide / dimethylformamide / 20 °C
With
tetra-(n-butyl)ammonium iodide; sodium hydride; sodium carbonate;
In
methanol; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 75 percent / lipase PS-30 / 1,2-dimethoxy-ethane / 14 h / 20 °C
2.1: 99 percent / SO3*pyridine; ethyldiisopropylamine / CH2Cl2; dimethylsulfoxide / 0 °C
3.1: sBuLi; (-)-(MeO)B(isopinocampheyl)2; BF3*OEt2 / tetrahydrofuran / 14 h / -78 °C
3.2: NaOH; H2O2 / H2O / -78 - 20 °C
4.1: sodium carbonate / methanol / 20 °C
5.1: 99 percent / sodium hydride; tetrabutylammonium iodide / dimethylformamide / 20 °C
With
lipase PS-30; pyridine-SO3 complex; boron trifluoride diethyl etherate; sec.-butyllithium; tetra-(n-butyl)ammonium iodide; sodium hydride; sodium carbonate; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide;
DOI:10.1002/anie.200604053
