2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Base Information

• Chemical Name: 2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate
• CAS No.: 1031364-55-2
• Molecular Formula: C₅₇H₈₅NO₂₂
• Molecular Weight: 1136.3

Synonyms:2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

Chemical Property of 2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

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Technology Process of 2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate

There total 9 articles about 2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

methyl 3-(CH2O[CH2CH2O]CH2CH2OMe)-4-hydroxy-5-methylbenzoate (1031364-35-8) + 2,7-(OMHEG)2-acridine-9-carboxylic acid (1031364-52-9) → 2,7-(OMHEG)2-2'-(CH2O[CH2CH2O]CH2CH2OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate (1031364-55-2)

Guidance literature:

2,7-(OMHEG)2-acridine-9-carboxylic acid; With pyridine; p-toluenesulfonyl chloride; at 20 ℃; for 0.166667h; Inert atmosphere;

methyl 3-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-4-hydroxy-5-methylbenzoate; at 20 ℃; for 72h;

Reference yield:

2,7-dimethoxy acridine-9-carboxylic acid (172834-75-2) → 2,7-(OMHEG)2-2'-(CH2O[CH2CH2O]CH2CH2OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate (1031364-55-2)

Guidance literature:

Multi-step reaction with 6 steps

1.1: thionyl chloride / 1 h / Reflux; Inert atmosphere

2.1: pyridine / 37 h / 0 - 20 °C

3.1: boron tribromide / dichloromethane / 48 h / 20 °C

3.2: 20 °C / Cooling with ice

4.1: caesium carbonate / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

5.1: potassium hydroxide; water / 16 h / 20 °C

6.1: pyridine; p-toluenesulfonyl chloride / 0.17 h / 20 °C / Inert atmosphere

6.2: 72 h / 20 °C

With pyridine; thionyl chloride; water; boron tribromide; caesium carbonate; p-toluenesulfonyl chloride; potassium hydroxide; In tetrahydrofuran; dichloromethane;

Reference yield:

C17H15NO4 (1031364-44-9) → 2,7-(OMHEG)2-2'-(CH2O[CH2CH2O]CH2CH2OMe)-4'-methoxycarbonylphenyl-6'-Me-acridine-9-carboxylate (1031364-55-2)

Guidance literature:

Multi-step reaction with 4 steps

1.1: boron tribromide / dichloromethane / 48 h / 20 °C

1.2: 20 °C / Cooling with ice

2.1: caesium carbonate / tetrahydrofuran / 4 h / Reflux; Inert atmosphere

3.1: potassium hydroxide; water / 16 h / 20 °C

4.1: pyridine; p-toluenesulfonyl chloride / 0.17 h / 20 °C / Inert atmosphere

4.2: 72 h / 20 °C

With pyridine; water; boron tribromide; caesium carbonate; p-toluenesulfonyl chloride; potassium hydroxide; In tetrahydrofuran; dichloromethane;

upstream raw materials:

2,7-dimethoxy acridine-9-carboxylic acid

C₁₆H₁₂ClNO₃

methyl 4-hydroxy-3,5-dimethylbenzoate

3,5-dimethyl-4-hydroxybenzoic acid

Downstream raw materials:

NSP-2,7-(OMHEG)2-2'-(CH₂O[CH₂CH₂O]CH₂CH₂OMe)-6'-Me-AE

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