Technology Process of C17H15NO2
There total 5 articles about C17H15NO2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
allyl(cyclopentadiene)palladium(II); tris(para-trifluoromethyl)phenyl phosphine;
In
dichloromethane;
at 40 ℃;
for 6h;
DOI:10.1039/c0cc05308b
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.05 h / -78 - 0 °C
1.2: 3 h / -78 °C
2.1: methanol; potassium carbonate / 1 h / 20 °C
3.1: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C
4.1: allyl(cyclopentadiene)palladium(II); tris(para-trifluoromethyl)phenyl phosphine / dichloromethane / 6 h / 40 °C
With
methanol; n-butyllithium; allyl(cyclopentadiene)palladium(II); potassium carbonate; triethylamine; tris(para-trifluoromethyl)phenyl phosphine;
In
tetrahydrofuran; hexane; dichloromethane;
1.1: Wittig reaction / 1.2: Wittig reaction;
DOI:10.1039/c0cc05308b
- Guidance literature:
-
Multi-step reaction with 3 steps
1: methanol; potassium carbonate / 1 h / 20 °C
2: triethylamine / dichloromethane / 2.5 h / 0 - 20 °C
3: allyl(cyclopentadiene)palladium(II); tris(para-trifluoromethyl)phenyl phosphine / dichloromethane / 6 h / 40 °C
With
methanol; allyl(cyclopentadiene)palladium(II); potassium carbonate; triethylamine; tris(para-trifluoromethyl)phenyl phosphine;
In
dichloromethane;
DOI:10.1039/c0cc05308b
