(5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid

Base Information

Chemical Name:(5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid
CAS No.:36954-80-0
Molecular Formula:C₁₇H₂₀N₂O₅S
Molecular Weight:364.422
Hs Code.:

(5<i>R</i>)-3,3,6<i>c</i>-trimethyl-7-oxo-6<i>t</i>-(2-phenoxy-acetylamino)-(5<i>r</i><i>H</i>)-4-thia-1-aza-bicyclo[3.2.0]heptane-2<i>c</i>-carboxylic acid

Synonyms:(5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid

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Chemical Property of (5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid

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Technology Process of (5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid

There total 6 articles about (5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36954-79-7
(5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid 4-methoxy-benzyl ester

: 36954-80-0
(5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid

Guidance literature:: With hydrogen; Lindlar's catalyst; In 1,4-dioxane; water; under 760 Torr; Ambient temperature;
DOI:10.1021/jo00942a008

Reference yield:

: 36955-05-2
(5R)-6t-benzylideneamino-3,3,6c-trimethyl-7-oxo-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid 4-methoxy-benzyl ester

: 36954-80-0
(5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid

Guidance literature:: Multi-step reaction with 3 steps

1: TsOH / ethyl acetate / Ambient temperature

2: Et₃N / CHCl₃

3: H₂ / Pd-CaCO₃ / dioxane; H₂O / 760 Torr / Ambient temperature

With hydrogen; toluene-4-sulfonic acid; triethylamine; Lindlar's catalyst; In 1,4-dioxane; chloroform; water; ethyl acetate;
DOI:10.1021/jo00942a008

Reference yield:

: 36954-78-6
(5R)-6t-amino-3,3,6c-trimethyl-7-oxo-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid 4-methoxy-benzyl ester

: 36954-80-0
(5R)-3,3,6c-trimethyl-7-oxo-6t-(2-phenoxy-acetylamino)-(5rH)-4-thia-1-aza-bicyclo[3.2.0]heptane-2c-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CHCl₃

2: H₂ / Pd-CaCO₃ / dioxane; H₂O / 760 Torr / Ambient temperature

With hydrogen; triethylamine; Lindlar's catalyst; In 1,4-dioxane; chloroform; water;
DOI:10.1021/jo00942a008