benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate

Base Information

Chemical Name:benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate
CAS No.:1181810-80-9
Molecular Formula:C₃₁H₃₄N₂O₆
Molecular Weight:530.621
Hs Code.:

Synonyms:benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate

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Chemical Property of benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate

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Technology Process of benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate

There total 6 articles about benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 791778-61-5
benzyl N-[2-((fluorenylmethoxycarbonyl)amino)ethyl]glycinate

: 1292200-60-2
N-tert-butoxycarbonyl-5-methylisocytosin-1-yl-acetic acid

: 1181810-80-9
benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate

Guidance literature:: With benzotriazol-1-ol; dicyclohexyl-carbodiimide; In tetrahydrofuran; water; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1016/j.bmcl.2011.01.130

Reference yield:

: 1292200-55-5
N₂-tert-butoxycarbonyl-5-methylisocytosine

: 1181810-80-9
benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate

Guidance literature:: Multi-step reaction with 3 steps

1.1: potassium carbonate / tetrahydrofuran / 0.5 h / Inert atmosphere

1.2: 20 °C / Inert atmosphere; Darkness

2.1: sodium hydroxide / tetrahydrofuran / 0.83 h / 0 °C / Inert atmosphere

3.1: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran; water / 0 - 20 °C / Inert atmosphere

With potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2011.01.130

Reference yield:

: 1292200-57-7
ethyl N₂-tert-butoxycarbonyl-5-methylisocytosin-1-yl-acetate

: 1181810-80-9
benzyl 2-((2-(((9H-fluoren-9-yl)methoxy)carbonylamino)ethyl)(tert-butoxycarbonyl)amino)acetate

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydroxide / tetrahydrofuran / 0.83 h / 0 °C / Inert atmosphere

2: benzotriazol-1-ol; dicyclohexyl-carbodiimide / tetrahydrofuran; water / 0 - 20 °C / Inert atmosphere

With benzotriazol-1-ol; dicyclohexyl-carbodiimide; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1016/j.bmcl.2011.01.130