tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate

Base Information

Chemical Name:tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate
CAS No.:645413-91-8
Molecular Formula:C₁₅H₂₀O₄
Molecular Weight:264.321
Hs Code.:

Synonyms:tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate

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Chemical Property of tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate

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Technology Process of tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate

There total 1 articles about tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 691-64-5
di-tert-butyl oxalate

: 14425-64-0
4-methoxyphenethyl bromide

: 645413-91-8
tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate

Guidance literature:: 4-methoxyphenethyl bromide; With iodine; magnesium; In diethyl ether; at 0 ℃; for 1.5h;

di-tert-butyl oxalate; In diethyl ether; dichloromethane; at -78 ℃; for 1.5h;
DOI:10.1021/ja909457b

Reference yield: 90.0%

: 645413-91-8
tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate

: 1393687-35-8
tert-butyl 2-amino-4-(4-methoxyphenyl)butanoate

Guidance literature:: tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate; With 2-Hydroxybenzylamine; triethylamine; In methanol; at 60 ℃; for 24h;

With hydrogenchloride; water; In tetrahydrofuran; at 20 ℃; for 5h;

With sodium hydrogencarbonate; In water; pH=8;
DOI:10.1016/j.tet.2012.06.023

Reference yield: 88.0%

: 645413-91-8
tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate

: 1402159-98-1
C₁₅H₂₃NO₃

Guidance literature:: tert-butyl 4-(4'-methoxyphenyl)-2-oxobutanoate; With C₄₃H₅₅N₃O₃S; 2-CHLOROBENZYLAMINE; In benzene; at 50 ℃; for 60h; Molecular sieve; Inert atmosphere; Schlenk technique;

With hydrogenchloride; In tetrahydrofuran; benzene; enantioselective reaction;
DOI:10.1021/ol302427d