octadec-9-enoic acid {3-hydroxy-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-3,6-dihydro-2H-pyran-2-ylmethyl}-amide

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Chemical Name:octadec-9-enoic acid {3-hydroxy-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-3,6-dihydro-2H-pyran-2-ylmethyl}-amide
CAS No.:350684-96-7
Molecular Formula:C₂₉H₄₉F₃N₂O₅
Molecular Weight:562.714
Hs Code.:

Synonyms:octadec-9-enoic acid {3-hydroxy-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-3,6-dihydro-2H-pyran-2-ylmethyl}-amide

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Chemical Property of octadec-9-enoic acid {3-hydroxy-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-3,6-dihydro-2H-pyran-2-ylmethyl}-amide

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Technology Process of octadec-9-enoic acid {3-hydroxy-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-3,6-dihydro-2H-pyran-2-ylmethyl}-amide

There total 1 articles about octadec-9-enoic acid {3-hydroxy-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-3,6-dihydro-2H-pyran-2-ylmethyl}-amide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78008-15-8
N-(3-hydroxypropyl)trifluoroacetamide

: 350684-96-7
octadec-9-enoic acid {3-hydroxy-6-[3-(2,2,2-trifluoro-acetylamino)-propoxy]-3,6-dihydro-2H-pyran-2-ylmethyl}-amide

Guidance literature:: Multi-step reaction with 6 steps

1.1: BF₃*Et₂O / CH₂Cl₂ / 1 h / 0 °C

2.1: MeONa / methanol / 0.25 h / 20 °C

3.1: 70 percent / pyridine / CH₂Cl₂ / 0 °C

4.1: 70 percent / NaN₃; NaI; 18-crown-6 / dimethylformamide / 60 °C

5.1: triphenylphosphine / tetrahydrofuran / 1 h / 30 - 40 °C

5.2: water / tetrahydrofuran / 2 h / 40 °C

6.1: 4.7 g / dicyclohexylcarbodiimide / CH₂Cl₂ / 2 h / 20 °C

With pyridine; sodium azide; 18-crown-6 ether; boron trifluoride diethyl etherate; sodium methylate; dicyclohexyl-carbodiimide; triphenylphosphine; sodium iodide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; 1.1: Ferrier condensation / 5.1: Staudinger reaction / 5.2: Staudinger reaction;
DOI:10.1021/ol0159423