ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate

Base Information

Chemical Name:ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate
CAS No.:705302-73-4
Molecular Formula:C₂₃H₂₃ClN₂O₆S
Molecular Weight:490.964
Hs Code.:

Synonyms:ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate

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Chemical Property of ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate

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Technology Process of ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate

There total 2 articles about ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 102153-63-9
6-chloronaphth-2-ylsulfonyl chloride

: ethyl (R)-3-amino-2-(benzyloxycarbonylamino)propionate hydrochloride

: 705302-73-4
ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate

Guidance literature:: With triethylamine; In dichloromethane; at 20 ℃; for 72h;
DOI:10.1248/cpb.52.459

Reference yield:

: 62234-37-1
2-(R)-amino>-3-aminopropionic acid

: 705302-73-4
ethyl (R)-2-(benzyloxycarbonyl)amino-3-[(6-chloro-2-naphthalenylsulfonyl)amino]propionate

Guidance literature:: Multi-step reaction with 2 steps

1: 87 percent / HCl / 20 °C

2: 97 percent / Et₃N / CH₂Cl₂ / 72 h / 20 °C

With hydrogenchloride; triethylamine; In dichloromethane;
DOI:10.1248/cpb.52.459