C₄₇H₇₁N₁₃O₉

Base Information

Chemical Name:C₄₇H₇₁N₁₃O₉
CAS No.:1431217-36-5
Molecular Formula:C₄₇H₇₁N₁₃O₉
Molecular Weight:962.162
Hs Code.:

C<sub>47</sub>H<sub>71</sub>N<sub>13</sub>O<sub>9</sub>

Synonyms:C₄₇H₇₁N₁₃O₉

Suppliers and Price of C₄₇H₇₁N₁₃O₉

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₄₇H₇₁N₁₃O₉

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₄₇H₇₁N₁₃O₉

There total 18 articles about C₄₇H₇₁N₁₃O₉ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1431217-35-4
C₆₅H₁₁₁N₁₃O₉Si₂

: 1431217-36-5
C₄₇H₇₁N₁₃O₉

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; methanol; for 3h;
DOI:10.1039/c3cc40628h

Reference yield:

: 22818-40-2
D-4-hydroxyphenylglycine

: 1431217-36-5
C₄₇H₇₁N₁₃O₉

Guidance literature:: Multi-step reaction with 11 steps

1.1: acetic acid; Iodine monochloride / 72 h / 20 °C / Inert atmosphere

2.1: triethylamine / water; 1,4-dioxane

2.2: pH 2 - 3

3.1: sodium hydroxide / dichloromethane; water / 3 h / 0 - 20 °C

3.2: pH 2 - 3

4.1: copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / 20 h / 20 °C / Inert atmosphere

5.1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

6.1: trifluoroacetic acid / dichloromethane / 1 h

7.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

8.1: dimethyl amine; 1-thiopropane / tetrahydrofuran / 1 h

9.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

10.1: potassium carbonate / acetone / 24 h

11.1: tetrabutyl ammonium fluoride / methanol; tetrahydrofuran / 3 h

With copper(l) iodide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; 1-thiopropane; tetrabutyl ammonium fluoride; Iodine monochloride; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dimethyl amine; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetone; 4.1: |Sonogashira Cross-Coupling;
DOI:10.1039/c3cc40628h

Reference yield:

: (R)-2-{[((9H-fluoren-9-yl)methoxy)carbonyl]amino}-6-azidohexanoic acid

: 1431217-36-5
C₄₇H₇₁N₁₃O₉

Guidance literature:: Multi-step reaction with 7 steps

1: (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

2: trifluoroacetic acid / dichloromethane / 1 h

3: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 4 h

4: dimethyl amine; 1-thiopropane / tetrahydrofuran / 1 h

5: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol; N-ethyl-N,N-diisopropylamine / dichloromethane / 3 h

6: potassium carbonate / acetone / 24 h

7: tetrabutyl ammonium fluoride / methanol; tetrahydrofuran / 3 h

With 1-thiopropane; tetrabutyl ammonium fluoride; potassium carbonate; (benzotriazo-1-yloxy)tris(dimethylamino)phosphonium hexafluorophosphate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; dimethyl amine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; In tetrahydrofuran; methanol; dichloromethane; acetone;
DOI:10.1039/c3cc40628h