4-cyanopentanoic acid diselenobenzoate

Base Information

• Chemical Name: 4-cyanopentanoic acid diselenobenzoate
• CAS No.: 1451203-74-9
• Molecular Formula: C₁₃H₁₃NO₂Se₂
• Molecular Weight: 373.172
• Mol file: 1451203-74-9.mol

Synonyms:4-cyanopentanoic acid diselenobenzoate

Chemical Property of 4-cyanopentanoic acid diselenobenzoate

Chemical Property:

Purity/Quality:

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Technology Process of 4-cyanopentanoic acid diselenobenzoate

There total 2 articles about 4-cyanopentanoic acid diselenobenzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C14H10Se4 + 4,4'-dicyano-4,4'-azo-di-valeric acid (2638-94-0,30248-30-7) → 4-cyanopentanoic acid diselenobenzoate (1451203-74-9)

Guidance literature:

In ethyl acetate; for 24h; Reflux;

DOI:10.1016/j.polymer.2013.07.060

Reference yield:

benzyl chloride (100-44-7) → 4-cyanopentanoic acid diselenobenzoate (1451203-74-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium methylate; selenium / methanol / 12 h / 20 - 67 °C / Inert atmosphere

1.2: 1 h

2.1: ethyl acetate / 24 h / Reflux

With selenium; sodium methylate; In methanol; ethyl acetate;

DOI:10.1016/j.polymer.2013.07.060

upstream raw materials:

4,4'-dicyano-4,4'-azo-di-valeric acid

benzyl chloride

Refernces