C₃₈H₃₇BrN₄O₁₀

Base Information

Chemical Name:C₃₈H₃₇BrN₄O₁₀
CAS No.:496789-57-2
Molecular Formula:C₃₈H₃₇BrN₄O₁₀
Molecular Weight:789.637
Hs Code.:

C<sub>38</sub>H<sub>37</sub>BrN<sub>4</sub>O<sub>10</sub>

Synonyms:C₃₈H₃₇BrN₄O₁₀

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Chemical Property of C₃₈H₃₇BrN₄O₁₀

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Technology Process of C₃₈H₃₇BrN₄O₁₀

There total 18 articles about C₃₈H₃₇BrN₄O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 793728-21-9
C₃₈H₃₇BrN₄O₉

: 496789-57-2
C₃₈H₃₇BrN₄O₁₀

Guidance literature:: With sodium chlorite; sodium dihydrogenphosphate; recorcinol; In dimethyl sulfoxide; at 25 ℃; for 2h;
DOI:10.1021/ja040092i

Reference yield:

: 13734-41-3
t-Boc-L-valine

: 496789-57-2
C₃₈H₃₇BrN₄O₁₀

Guidance literature:: Multi-step reaction with 16 steps

1.1: 92 percent / EDC*H₂O; HOBt*H₂O; Et₃N / CH₂Cl₂ / 12 h / 25 °C

2.1: 80 percent / Burgess reagent / tetrahydrofuran / 4 h / Heating

3.1: 90 percent / DBU; BrCCl₃ / CH₂Cl₂ / 3 h / 25 °C

4.1: 83 percent / LiBH₄ / ethanol; tetrahydrofuran / 0 - 25 °C

5.1: NaHMDS / tetrahydrofuran / -78 °C

5.2: 72 percent / n-tetrabutylammonium iodide / tetrahydrofuran / 36 h / 25 °C

6.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

6.2: 73 percent / tetrahydrofuran; hexane / 0.08 h / -78 °C

7.1: 47 percent / p-toluenesulfonic acid monohydrate / 1,2-dichloro-ethane / 0.42 h / Heating

8.1: 4.6 g / aq. NaHCO₃ / dioxane / 2 h / 25 °C

9.1: 85 percent / K₂CO₃ / acetone / 0 - 25 °C

10.1: aq. LiOH / tetrahydrofuran; methanol / 0.33 h / Heating

11.1: trifluoroacetic acid / 0.17 h

12.1: 0.220 g / HATU; 2,4,6-collidine / CH₂Cl₂; dimethylformamide / 12 h / 25 °C

13.1: 65 percent / BCl₃ / CH₂Cl₂ / 2 h / -78 °C

14.1: 70 percent / Et₃N; 4-dimethylaminopyridine / dioxane / 1 h / 25 °C

15.1: 1-hydroxy-1,2-benziodoxol-3(1H)-one / dimethylsulfoxide / 2 h / 25 °C

16.1: 0.072 g / NaClO₂; resorcinol; aq. NaH₂PO₄ / dimethylsulfoxide / 2 h / 25 °C

With 2,4,6-trimethyl-pyridine; dmap; lithium hydroxide; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; n-butyllithium; 1-hydroxy-1,2-benzodioxol-3-(1H)-one; Burgess Reagent; Bromotrichloromethane; sodium hexamethyldisilazane; boron trichloride; sodium hydrogencarbonate; potassium carbonate; benzotriazol-1-ol; toluene-4-sulfonic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; recorcinol; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja040092i

Reference yield:

: 158068-97-4
2-<(S)-1--2-methylpropyl>-4-carbomethoxyoxazole

: 496789-57-2
C₃₈H₃₇BrN₄O₁₀

Guidance literature:: Multi-step reaction with 13 steps

1.1: 83 percent / LiBH₄ / ethanol; tetrahydrofuran / 0 - 25 °C

2.1: NaHMDS / tetrahydrofuran / -78 °C

2.2: 72 percent / n-tetrabutylammonium iodide / tetrahydrofuran / 36 h / 25 °C

3.1: n-BuLi / tetrahydrofuran; hexane / 0.5 h / -78 °C

3.2: 73 percent / tetrahydrofuran; hexane / 0.08 h / -78 °C

4.1: 47 percent / p-toluenesulfonic acid monohydrate / 1,2-dichloro-ethane / 0.42 h / Heating

5.1: 4.6 g / aq. NaHCO₃ / dioxane / 2 h / 25 °C

6.1: 85 percent / K₂CO₃ / acetone / 0 - 25 °C

7.1: aq. LiOH / tetrahydrofuran; methanol / 0.33 h / Heating

8.1: trifluoroacetic acid / 0.17 h

9.1: 0.220 g / HATU; 2,4,6-collidine / CH₂Cl₂; dimethylformamide / 12 h / 25 °C

10.1: 65 percent / BCl₃ / CH₂Cl₂ / 2 h / -78 °C

11.1: 70 percent / Et₃N; 4-dimethylaminopyridine / dioxane / 1 h / 25 °C

12.1: 1-hydroxy-1,2-benziodoxol-3(1H)-one / dimethylsulfoxide / 2 h / 25 °C

13.1: 0.072 g / NaClO₂; resorcinol; aq. NaH₂PO₄ / dimethylsulfoxide / 2 h / 25 °C

With 2,4,6-trimethyl-pyridine; dmap; lithium hydroxide; sodium chlorite; sodium dihydrogenphosphate; lithium borohydride; n-butyllithium; 1-hydroxy-1,2-benzodioxol-3-(1H)-one; sodium hexamethyldisilazane; boron trichloride; sodium hydrogencarbonate; potassium carbonate; toluene-4-sulfonic acid; triethylamine; trifluoroacetic acid; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; recorcinol; In tetrahydrofuran; 1,4-dioxane; methanol; ethanol; hexane; dichloromethane; dimethyl sulfoxide; 1,2-dichloro-ethane; N,N-dimethyl-formamide; acetone;
DOI:10.1021/ja040092i