dibenzyl phosphorofluoridate

Base Information

• Chemical Name: dibenzyl phosphorofluoridate
• CAS No.: 123417-05-0
• Molecular Formula: C₁₄H₁₄FO₃P
• Molecular Weight: 280.236
• Mol file: 123417-05-0.mol

Synonyms:dibenzyl phosphorofluoridate

Chemical Property of dibenzyl phosphorofluoridate

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

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Technology Process of dibenzyl phosphorofluoridate

There total 2 articles about dibenzyl phosphorofluoridate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

phosphoric acid dibenzyl ester (1623-08-1) → dibenzyl phosphorofluoridate (123417-05-0)

Guidance literature:

With 2-fluoro 4-methyl pyridinium tosylate; triethylamine;

DOI:10.1016/S0040-4039(00)82184-X

Reference yield: 80.0%

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate (990-91-0) → dibenzyl phosphorofluoridate (123417-05-0)

Guidance literature:

With cesium fluoride; In acetonitrile; Ambient temperature;

DOI:10.1016/S0040-4039(00)82184-X

Reference yield: 100.0%

2-Chlorobenzyl alcohol (17849-38-6) + dibenzyl phosphorofluoridate (123417-05-0) → Phosphoric acid dibenzyl ester 2-chloro-benzyl ester (136815-44-6)

Guidance literature:

With cesium fluoride; In acetonitrile; for 18h; Product distribution; Ambient temperature; var. alcohols and phenols; var. base: DBU, n-BuLi;

DOI:10.1016/S0040-4039(00)82184-X

upstream raw materials:

phosphoric acid dibenzyl ester

dibenzyl [[bis(benzyloxy)phosphoryl]oxy]phosphonate

Downstream raw materials:

(+/-)dibenzyl (2,2-dimethyl-1,3-dioxolan-4-yl)methyl phosphate

phosphoric Acid dibenzyl ester octadecyl ester

Phosphoric acid dibenzyl ester (3R,4S,5R,6R)-3,4,5-tris-benzyloxy-6-benzyloxymethyl-tetrahydro-pyran-2-yl ester

3-(dibenzyl)phosphoryloxy-1-methyl-1-propanol