3'-O-Demethylarctigenin

Base Information

Chemical Name:3'-O-Demethylarctigenin
CAS No.:147022-95-5
Molecular Formula:C₂₀H₂₂O₆
Molecular Weight:358.391
Hs Code.:
Mol file:147022-95-5.mol

Synonyms:PP-6 (Piper philippinum)

Suppliers and Price of 3'-O-Demethylarctigenin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Arctom
3'-O-Demethylarctigenin
5mg
$ 468.00

Total 6 raw suppliers

Chemical Property of 3'-O-Demethylarctigenin

Chemical Property:

Purity/Quality:

Analysis control,HPLC≥95% ^*data from raw suppliers

3'-O-Demethylarctigenin ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3'-O-Demethylarctigenin

There total 6 articles about 3'-O-Demethylarctigenin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 26687-82-1,81446-30-2,84413-77-4,87678-74-8,87678-75-9,144901-91-7,7770-78-7
Arctigenin

: 147022-95-5
PP-6 (Piper philippinum)

Guidance literature:: With pyridine; aluminum (III) chloride; In dichloromethane; for 20h; Reflux;
DOI:10.1016/j.ejmech.2012.11.031

Reference yield:

: (R)-4-benzyl-3-[(S)-2-[(R)-(3,4-dimethoxyphenyl)(hydroxy)methyl]-4-pentenoyl-2-oxazolidinone]

: 147022-95-5
PP-6 (Piper philippinum)

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylsilane; boron trifluoride diethyl etherate / dichloromethane / 1 h / 0 °C

2.1: lithium borohydride / methanol / 0.5 h / 20 °C

3.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tert-butyl alcohol; water / 72 h / 20 °C

3.2: 2 h / 20 °C

3.3: Molecular sieve

4.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 20 °C

With triethylsilane; osmium(VIII) oxide; lithium borohydride; 5%-palladium/activated carbon; boron trifluoride diethyl etherate; hydrogen; 4-methylmorpholine N-oxide; In methanol; dichloromethane; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2020.127191

Reference yield:

: (R)-4-benzyl-3-[(S)-2-(3,4-dimethoxybenzyl)-4-pentenoyl]-2-oxazolidinone

: 147022-95-5
PP-6 (Piper philippinum)

Guidance literature:: Multi-step reaction with 3 steps

1.1: lithium borohydride / methanol / 0.5 h / 20 °C

2.1: 4-methylmorpholine N-oxide; osmium(VIII) oxide / tert-butyl alcohol; water / 72 h / 20 °C

2.2: 2 h / 20 °C

2.3: Molecular sieve

3.1: 5%-palladium/activated carbon; hydrogen / ethyl acetate / 20 °C

With osmium(VIII) oxide; lithium borohydride; 5%-palladium/activated carbon; hydrogen; 4-methylmorpholine N-oxide; In methanol; water; ethyl acetate; tert-butyl alcohol;
DOI:10.1016/j.bmcl.2020.127191