C₃₃H₃₂ClFN₄O₁₁S

Base Information

Chemical Name:C₃₃H₃₂ClFN₄O₁₁S
CAS No.:1417792-22-3
Molecular Formula:C₃₃H₃₂ClFN₄O₁₁S
Molecular Weight:747.155
Hs Code.:

C<sub>33</sub>H<sub>32</sub>ClFN<sub>4</sub>O<sub>11</sub>S

Synonyms:C₃₃H₃₂ClFN₄O₁₁S

Suppliers and Price of C₃₃H₃₂ClFN₄O₁₁S

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₃₂ClFN₄O₁₁S

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₃₂ClFN₄O₁₁S

There total 14 articles about C₃₃H₃₂ClFN₄O₁₁S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 1417792-27-8
C₃₅H₃₆ClFN₄O₁₁S

: 1417792-22-3
C₃₃H₃₂ClFN₄O₁₁S

Guidance literature:: With water; potassium carbonate; In methanol; at 80 ℃; for 0.0833333h;
DOI:10.1021/jm3014844

Reference yield:

: 1417792-28-9
C₁₃H₁₁FN₂O₂

: 1417792-22-3
C₃₃H₃₂ClFN₄O₁₁S

Guidance literature:: Multi-step reaction with 7 steps

1: dichloromethane / 0.08 h / Molecular sieve

2: sodium tris(acetoxy)borohydride / dichloromethane / 2 h / 20 °C

3: zinc; ammonium chloride / water; acetone / 0.17 h / 20 °C

4: hydrogenchloride / methanol / 0.17 h / 60 °C

5: triethylamine / tetrahydrofuran / 0 °C

6: triethylamine / tetrahydrofuran / 0.08 h / 100 °C

7: potassium carbonate; water / methanol / 0.08 h / 80 °C

With hydrogenchloride; water; sodium tris(acetoxy)borohydride; potassium carbonate; ammonium chloride; triethylamine; zinc; In tetrahydrofuran; methanol; dichloromethane; water; acetone;
DOI:10.1021/jm3014844

Reference yield:

: 73781-91-6
6-Chloronicotinic acid methyl ester

: 1417792-22-3
C₃₃H₃₂ClFN₄O₁₁S

Guidance literature:: Multi-step reaction with 8 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾ / 1,4-dioxane; water / 0.25 h / 100 °C

2: dichloromethane / 0.08 h / Molecular sieve

3: sodium tris(acetoxy)borohydride / dichloromethane / 2 h / 20 °C

4: zinc; ammonium chloride / water; acetone / 0.17 h / 20 °C

5: hydrogenchloride / methanol / 0.17 h / 60 °C

6: triethylamine / tetrahydrofuran / 0 °C

7: triethylamine / tetrahydrofuran / 0.08 h / 100 °C

8: potassium carbonate; water / methanol / 0.08 h / 80 °C

With hydrogenchloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; water; sodium tris(acetoxy)borohydride; potassium carbonate; ammonium chloride; triethylamine; zinc; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; acetone; 1: |Suzuki Coupling;
DOI:10.1021/jm3014844