bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane

Base Information

Chemical Name:bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane
CAS No.:1440146-87-1
Molecular Formula:C₃₂H₆₀O₆Si₅
Molecular Weight:681.252
Hs Code.:

Synonyms:bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane

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Chemical Property of bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane

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Technology Process of bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane

There total 3 articles about bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.0%

: 1253730-12-9
(chloromethyl)dimethyl(2,4,6-trimethoxyphenyl)silane

: 2295-07-0
bis[(chlorodimethylsilyl)methyl]dimethylsilane

: 1440146-87-1
bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane

Guidance literature:: (chloromethyl)dimethyl(2,4,6-trimethoxyphenyl)silane; With naphthalene; lithium; In tetrahydrofuran; at -30 - 20 ℃; for 18h; Inert atmosphere;

bis[(chlorodimethylsilyl)methyl]dimethylsilane; In tetrahydrofuran; at -30 ℃; for 1h; Inert atmosphere;
DOI:10.1021/om400190q

Reference yield:

: 621-23-8
1,2,3-trimethoxybenzene

: 1440146-87-1
bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: n-butyllithium; N,N,N,N,-tetramethylethylenediamine / pentane; hexane / 3.5 h / 0 - 20 °C / Inert atmosphere

1.2: 18 h / 0 - 20 °C / Inert atmosphere

2.1: naphthalene; lithium / tetrahydrofuran / 18 h / -30 - 20 °C / Inert atmosphere

2.2: 1 h / -30 °C / Inert atmosphere

With n-butyllithium; naphthalene; N,N,N,N,-tetramethylethylenediamine; lithium; In tetrahydrofuran; hexane; pentane;
DOI:10.1021/om400190q

Reference yield:

: 1440146-84-8
bis[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilane

: 1440146-87-1
bis[[[[dimethyl(2,4,6-trimethoxyphenyl)silyl]methyl]dimethylsilyl]methyl]dimethylsilane

Guidance literature:: Multi-step reaction with 2 steps

1.1: hydrogenchloride / diethyl ether / 3.3 h / 0 - 20 °C / Inert atmosphere

2.1: naphthalene; lithium / tetrahydrofuran / 18 h / -30 - 20 °C / Inert atmosphere

2.2: 1 h / -30 °C / Inert atmosphere

With hydrogenchloride; naphthalene; lithium; In tetrahydrofuran; diethyl ether;
DOI:10.1021/om400190q