4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy

Base Information

Chemical Name:4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy
CAS No.:1227401-69-5
Molecular Formula:C₅₂H₄₆BN₃
Molecular Weight:723.768
Hs Code.:

4-( p-BMes<sub>2</sub>-phenyl)-4'-( p-NPh<sub>2</sub>-phenyl)-2,2'-bipy

Synonyms:4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy

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Chemical Property of 4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy

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Technology Process of 4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy

There total 1 articles about 4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 1227401-68-4
4-Br-4'-(p-NPh₂-phenyl)-2,2'-bipyridine

: 38186-40-2
p-bromophenyldimesitylborane

: 1227401-69-5
4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy

Guidance literature:: p-bromophenyldimesitylborane; With n-butyllithium; In tetrahydrofuran; at -78 ℃; for 1h;

With zinc(II) chloride; In tetrahydrofuran; at -78 - 20 ℃;

4-Br-4'-(p-NPh₂-phenyl)-2,2'-bipyridine; With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 55 ℃; for 48h;
DOI:10.1021/ic1004159

Reference yield: 71.0%

: 1227401-69-5
4-( p-BMes₂-phenyl)-4'-( p-NPh₂-phenyl)-2,2'-bipy

: 1227401-73-1
Pt(C₆H₅)2(C₁₀H₆N₂(C₆H₄B(C₆H₂(CH₃)3)2)C₆H₄N(C₆H₅)2)

Guidance literature:: With (Pt(C6H5)2(μ-SMe2)](n) n=2 or 3; In dichloromethane; (N2, Schlenk) a soln. of Pt-complex and bipyridine-compound in CH2Cl2 was stirred for 12 h under N2 at room temp.; the solvent was removed, the residue was washed with diethyl ether and dried under vac.; elem. anal.;
DOI:10.1021/ic1004159