(R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid

Base Information

Chemical Name:(R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid
CAS No.:155442-91-4
Molecular Formula:C₁₀H₁₀BrNO₃
Molecular Weight:272.098
Hs Code.:

Synonyms:(R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid

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Chemical Property of (R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid

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Technology Process of (R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid

There total 3 articles about (R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: sodium (4S)-4,5-dihydro-2-phenyloxazole-4-carboxylate

: 155442-91-4
(R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid

Guidance literature:: With trimethylsilyl bromide; water; In chloroform; at 20 ℃; for 48h;
DOI:10.1016/S0040-4039(01)00650-5

Reference yield:

: 78715-83-0
methyl (S)-2-phenyl-4,5-dihydrooxazole-4-carboxylate

: 155442-91-4
(R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / aq. NaOH / 3 h / 20 °C

2: Me₃SiBr / H₂O; CHCl₃ / 48 h / 20 °C

With sodium hydroxide; trimethylsilyl bromide; In chloroform; water;
DOI:10.1016/S0957-4166(03)00484-1

Reference yield:

: 5333-86-8
ethyl benzimidate hydrochloride

: 155442-91-4
(R)-(-)-2-(N-benzoyl-amino)-3-bromo propanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1.1: Et₃N / CHCl₃ / 20 °C

1.2: 80 percent / CHCl₃ / 24 h / Heating

2.1: 99 percent / aq. NaOH / 3 h / 20 °C

3.1: Me₃SiBr / H₂O; CHCl₃ / 48 h / 20 °C

With sodium hydroxide; trimethylsilyl bromide; triethylamine; In chloroform; water;
DOI:10.1016/S0957-4166(03)00484-1