C₁₂H₁₃ClO

Base Information

Chemical Name:C₁₂H₁₃ClO
CAS No.:1449549-06-7
Molecular Formula:C₁₂H₁₃ClO
Molecular Weight:208.688
Hs Code.:

Synonyms:C₁₂H₁₃ClO

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₂H₁₃ClO

Chemical Property:

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Technology Process of C₁₂H₁₃ClO

There total 2 articles about C₁₂H₁₃ClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 73383-23-0
1,1-dibromo 1-hexene

: 106-48-9,82344-39-6
4-chloro-phenol

: 1449549-06-7
C₁₂H₁₃ClO

Guidance literature:: 1,1-dibromo 1-hexene; 4-chloro-phenol; With [2,2]bipyridinyl; potassium phosphate; copper(l) iodide; at 110 ℃; for 48h; Inert atmosphere; Sealed tube;

With potassium tert-butylate; In 1,4-dioxane; at 20 ℃; Inert atmosphere;
DOI:10.1021/acs.joc.6b00535

Reference yield:

: 110-62-3
pentanal

: 1449549-06-7
C₁₂H₁₃ClO

Guidance literature:: Multi-step reaction with 2 steps

1.1: triphenylphosphine / dichloromethane / 0.5 h / 0 °C / Inert atmosphere

1.2: 1.08 h / 0 °C / Inert atmosphere

2.1: [2,2]bipyridinyl; potassium phosphate; copper(l) iodide / 48 h / 110 °C / Inert atmosphere; Sealed tube

2.2: 20 °C / Inert atmosphere

With [2,2]bipyridinyl; potassium phosphate; copper(l) iodide; triphenylphosphine; In dichloromethane;
DOI:10.1021/acs.joc.6b00535

Reference yield: 90.0%

: 591-50-4
iodobenzene

: 1449549-06-7
C₁₂H₁₃ClO

: C₁₈H₁₉ClO

Guidance literature:: With palladium diacetate; caesium carbonate; isopropyl alcohol; tricyclohexylphosphine tetrafluoroborate; In 1,4-dioxane; at 50 ℃; for 10h; regioselective reaction; Inert atmosphere;
DOI:10.1021/jo5002356