(S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol

Base Information

Chemical Name:(S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol
CAS No.:663599-85-7
Molecular Formula:C₂₈H₃₈O₄
Molecular Weight:438.607
Hs Code.:

Synonyms:(S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol

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Chemical Property of (S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol

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Technology Process of (S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol

There total 7 articles about (S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 663599-90-4
(S)-3-{(R)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propionyl}-4-isopropyl-oxazolidin-2-one

: 663599-85-7
(S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol

Guidance literature:: With sodium tetrahydroborate; In tetrahydrofuran; water;

Reference yield:

: 17123-60-3
2-methylhexa-1,5-dien-3-ol

: 663599-85-7
(S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol

Guidance literature:: Multi-step reaction with 7 steps

1: 43 percent / (-)-dicyclohexyl tartarate; Ti (OiPr)4; t-BuOOH / CH₂Cl₂

2: 87 percent / NaH / tetrahydrofuran

3: 86 percent / CuI / tetrahydrofuran / -20 °C

4: 87 percent / NaH / tetrahydrofuran

5: 85 percent / Me₃CCOCl; Et₃N / tetrahydrofuran / -78 - 0 °C

6: 70 percent / NaN(SiMe₃)2 / tetrahydrofuran / -78 °C

7: 88 percent / NaBH₄ / tetrahydrofuran; H₂O

With titanium(IV) isopropylate; tert.-butylhydroperoxide; sodium tetrahydroborate; copper(l) iodide; (-)-dicyclohexyl D-tartrate; sodium hexamethyldisilazane; pivaloyl chloride; sodium hydride; triethylamine; In tetrahydrofuran; dichloromethane; water;

Reference yield:

: 663599-88-0
(R)-1-((S)-2-Methyl-oxiranyl)-but-3-en-1-ol

: 663599-85-7
(S)-3-Benzyloxy-2-[(S)-1-((R)-1-benzyloxy-but-3-enyl)-1,4-dimethyl-pent-3-enyloxy]-propan-1-ol

Guidance literature:: Multi-step reaction with 6 steps

1: 87 percent / NaH / tetrahydrofuran

2: 86 percent / CuI / tetrahydrofuran / -20 °C

3: 87 percent / NaH / tetrahydrofuran

4: 85 percent / Me₃CCOCl; Et₃N / tetrahydrofuran / -78 - 0 °C

5: 70 percent / NaN(SiMe₃)2 / tetrahydrofuran / -78 °C

6: 88 percent / NaBH₄ / tetrahydrofuran; H₂O

With sodium tetrahydroborate; copper(l) iodide; sodium hexamethyldisilazane; pivaloyl chloride; sodium hydride; triethylamine; In tetrahydrofuran; water;