9-(methylthiomethyl)-9-borabicyclo{3.3.1}nonane dimer

Base Information

Chemical Name:9-(methylthiomethyl)-9-borabicyclo{3.3.1}nonane dimer
CAS No.:114614-14-1
Molecular Formula:C₂₀H₃₈B₂S₂
Molecular Weight:364.276
Hs Code.:

Synonyms:9-(methylthiomethyl)-9-borabicyclo{3.3.1}nonane dimer

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-(methylthiomethyl)-9-borabicyclo{3.3.1}nonane dimer

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Technology Process of 9-(methylthiomethyl)-9-borabicyclo{3.3.1}nonane dimer

There total 1 articles about 9-(methylthiomethyl)-9-borabicyclo{3.3.1}nonane dimer which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 114595-57-2
triphenylphosphine monomethylthiomethyborane adduct

: 5259-72-3,10060-40-9,111-78-4
cyclo-octa-1,5-diene

: 114614-14-1
9-(methylthiomethyl)-9-borabicyclo{3.3.1}nonane dimer

: 2065-66-9
methyl-triphenylphosphonium iodide

Guidance literature:: With methyl iodide; In tetrahydrofuran; moisture and air-oxygen exclusion, heating of B-compound and 20% excess COD in THF (60°C, 48 h), MeI addn., stirring (room temp., 24 h); removal of pptd. MePPh3I (filtn.), solvent removal, sublimation;