2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride

Base Information

Chemical Name:2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride
CAS No.:531507-38-7
Molecular Formula:C₁₀H₅Cl₂N₃O₃
Molecular Weight:286.074
Hs Code.:

Synonyms:2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride

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Chemical Property of 2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride

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Technology Process of 2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride

There total 3 articles about 2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 524712-41-2
2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoic acid

: 531507-38-7
2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride

Guidance literature:: With oxalyl dichloride; In dichloromethane;
DOI:10.1016/j.bmcl.2011.04.077

Reference yield:

: 524712-40-1
C₁₁H₆ClN₃O₆

: 531507-38-7
2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride

Guidance literature:: Multi-step reaction with 2 steps

1: mercaptoacetic acid; sodium hydroxide / water / 175 °C

2: oxalyl dichloride / dichloromethane

With oxalyl dichloride; mercaptoacetic acid; sodium hydroxide; In dichloromethane; water;
DOI:10.1016/j.bmcl.2011.04.077

Reference yield:

: 89-54-3
2-chloro-5-aminobenzoic acid

: 531507-38-7
2-chloro-5-(3,5-dioxo-4,5-dihydro-3H-[1,2,4]triazin-2-yl)-benzoyl chloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: hydrogenchloride; acetic acid; sodium nitrite / 0.5 h / 10 - 15 °C

1.2: 1.33 h / 10 - 20 °C

2.1: mercaptoacetic acid; sodium hydroxide / water / 175 °C

3.1: oxalyl dichloride / dichloromethane

With hydrogenchloride; oxalyl dichloride; acetic acid; mercaptoacetic acid; sodium hydroxide; sodium nitrite; In dichloromethane; water;
DOI:10.1016/j.bmcl.2011.04.077