tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical

Base Information

• Chemical Name: tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical
• CAS No.: 939824-22-3
• Molecular Formula: C₁₉Cl₁₂N₃O₆
• Molecular Weight: 791.661
• Mol file: 939824-22-3.mol

Synonyms:tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical

Chemical Property of tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical

There total 2 articles about tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

tris(2,3,5,6-tetrachloro-4-nitrophenyl)methane → tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical (939824-22-3)

Guidance literature:

tris(2,3,5,6-tetrachloro-4-nitrophenyl)methane; With tetra(n-butyl)ammonium hydroxide; In tetrahydrofuran; at 0 ℃; for 2h;

In tetrahydrofuran; at 0 ℃; for 0.5h; Further stages.;

DOI:10.1021/jo062665a

Reference yield:

Tris<2,3,5,6-tetrachlorophenyl>methane (105633-26-9) → tris(2,3,5,6-tetrachloro-4-nitrophenyl)methyl radical (939824-22-3)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 62 percent / nitric acid / 18 h / Heating

2.1: tetrabutylammonium hydroxide / tetrahydrofuran / 2 h / 0 °C

2.2: 48 percent / tetrachloro-p-quinone / tetrahydrofuran / 0.5 h / 0 °C

With tetra(n-butyl)ammonium hydroxide; nitric acid; In tetrahydrofuran;

DOI:10.1021/jo062665a

upstream raw materials:

Tris<2,3,5,6-tetrachlorophenyl>methane