(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

Base Information

Chemical Name:(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester
CAS No.:118715-41-6
Molecular Formula:C₃₂H₄₈O₉Si
Molecular Weight:604.813
Hs Code.:

Synonyms:(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

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Chemical Property of (S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

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Technology Process of (S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

There total 2 articles about (S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1139-97-5,1139-98-6,1851-12-3,3353-52-4,6163-35-5,14184-49-7,19146-17-9,22248-57-3,34361-56-3,34361-57-4,57793-53-0,7506-68-5
2,3,4,6-tetra-O-methyl-D-glucopyranose

: 118715-38-1
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid

: 118715-41-6
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

: 118715-40-5
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2R,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

Guidance literature:: With trichloroacetonitrile; sodium hydride; Yield given. Multistep reaction. Yields of byproduct given; 1.) CH₂Cl₂, 25 deg C, 2.) CH₂Cl₂;
DOI:10.1021/ja00186a037

Reference yield:

: 1139-97-5,1139-98-6,1851-12-3,3353-52-4,6163-35-5,14184-49-7,19146-17-9,22248-57-3,34361-56-3,34361-57-4,57793-53-0,7506-68-5
2,3,4,6-tetra-O-methyl-D-glucopyranose

: 118715-39-2
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanethioic acid S-(3-nitro-pyridin-2-yl) ester

: 118715-41-6
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2S,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

: 118715-40-5
(S)-4-(tert-Butyl-diphenyl-silanyloxy)-5-methoxy-pentanoic acid (2R,3R,4S,5R,6R)-3,4,5-trimethoxy-6-methoxymethyl-tetrahydro-pyran-2-yl ester

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1.) THF, -78 deg C;
DOI:10.1021/ja00186a037