C₃₂H₃₉N₃O₅

Base Information

• Chemical Name: C₃₂H₃₉N₃O₅
• CAS No.: 947490-51-9
• Molecular Formula: C₃₂H₃₉N₃O₅
• Molecular Weight: 545.679
• Mol file: 947490-51-9.mol

Synonyms:C₃₂H₃₉N₃O₅

Chemical Property of C₃₂H₃₉N₃O₅

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₃₂H₃₉N₃O₅

There total 3 articles about C₃₂H₃₉N₃O₅ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

C39H45N3O5 (947490-47-3) → C32H39N3O5 (947490-51-9)

Guidance literature:

C₃₉H₄₅N₃O₅; With acetic anhydride; acetic acid; zinc(II) chloride; at 20 ℃; for 5h;

With sodium methylate; In methanol; at 20 ℃; pH=10; Further stages.;

DOI:10.1039/b705750d

Reference yield:

C39H46O6 (947490-44-0) → C32H39N3O5 (947490-51-9)

Guidance literature:

Multi-step reaction with 2 steps

1.1: 92 percent / hydrazoic acid; DEAD; triphenylphosphine / toluene / 1 h / 20 °C

2.1: AcOH; Ac₂O; ZnCl₂ / 5 h / 20 °C

2.2: 81 percent / NaOMe / methanol / 20 °C / pH 10

With hydrogen azide; acetic anhydride; acetic acid; triphenylphosphine; zinc(II) chloride; diethylazodicarboxylate; In toluene;

DOI:10.1039/b705750d

Reference yield:

2,3,4,6-tetra-O-benzyl-1-formyl-D-glucopyranose (113019-43-5,140397-45-1,140397-46-2,140397-47-3,140397-49-5,91738-17-9) → C32H39N3O5 (947490-51-9)

Guidance literature:

Multi-step reaction with 3 steps

1.1: 48 percent / tetrahydrofuran; diethyl ether / 0 °C

2.1: 92 percent / hydrazoic acid; DEAD; triphenylphosphine / toluene / 1 h / 20 °C

3.1: AcOH; Ac₂O; ZnCl₂ / 5 h / 20 °C

3.2: 81 percent / NaOMe / methanol / 20 °C / pH 10

With hydrogen azide; acetic anhydride; acetic acid; triphenylphosphine; zinc(II) chloride; diethylazodicarboxylate; In tetrahydrofuran; diethyl ether; toluene;

DOI:10.1039/b705750d

upstream raw materials:

C₃₉H₄₅N₃O₅

C₃₉H₄₆O₆

2,3,4,6-tetra-O-benzyl-1-formyl-D-glucopyranose