Boc-cyclo-OMe

Base Information

Chemical Name:Boc-cyclo-OMe
CAS No.:153824-52-3
Molecular Formula:C₂₇H₄₀N₄O₇S₂
Molecular Weight:596.769
Hs Code.:

Synonyms:Boc-cyclo-OMe

Suppliers and Price of Boc-cyclo-OMe

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Boc-cyclo-OMe

Chemical Property:

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Technology Process of Boc-cyclo-OMe

There total 7 articles about Boc-cyclo-OMe which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 153824-51-2
Boc-Cys(Trt)-Leu-Phe-Cys(Acm)-OMe

: 153824-52-3
Boc-cyclo-OMe

Guidance literature:: With iodine; In methanol;
DOI:10.1002/ardp.19933261208

Reference yield:

: 13139-15-6,53296-34-7
N-tert-butoxycarbonyl-L-leucine

: 153824-52-3
Boc-cyclo-OMe

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) 95percent isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) CH₂Cl₂, -15 deg C, 10 min, 2.) CH₂Cl₂, DMF, -15 deg C, 15 min; r.t., overnight

2: HCl / tetrahydrofuran

3: 1.) 95percent isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) CH₂Cl₂, -15 deg C, 10 min, 2.) CH₂Cl₂, DMF, -15 deg C, 15 min; r.t., overnight

4: 94 percent / I₂ / methanol

With 4-methyl-morpholine; hydrogenchloride; iodine; isobutyl chloroformate; In tetrahydrofuran; methanol;
DOI:10.1002/ardp.19933261208

Reference yield:

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 153824-52-3
Boc-cyclo-OMe

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) 95percent isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) CH₂Cl₂, -15 deg C, 10 min, 2.) CH₂Cl₂, DMF, -15 deg C, 15 min; r.t., overnight

2: HCl / tetrahydrofuran

3: 1.) 95percent isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) CH₂Cl₂, -15 deg C, 10 min, 2.) CH₂Cl₂, DMF, -15 deg C, 15 min; r.t., overnight

4: HCl / tetrahydrofuran

5: 1.) 95percent isobutyl chloroformate, N-methylmorpholine, 2.) N-methylmorpholine / 1.) CH₂Cl₂, -15 deg C, 10 min, 2.) CH₂Cl₂, DMF, -15 deg C, 15 min; r.t., overnight

6: 94 percent / I₂ / methanol

With 4-methyl-morpholine; hydrogenchloride; iodine; isobutyl chloroformate; In tetrahydrofuran; methanol;
DOI:10.1002/ardp.19933261208