N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide

Base Information

Chemical Name:N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide
CAS No.:247031-67-0
Molecular Formula:C₁₇H₁₈N₂O₄S₂
Molecular Weight:378.473
Hs Code.:

Synonyms:N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide

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Chemical Property of N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide

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Technology Process of N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide

There total 4 articles about N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 107-20-0
2-chloroethanal

: 247031-65-8
N-[[(3-methoxyphenyl)amino]thioxomethyl]-4-methylphenylsulfonamide

: 247031-67-0
N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide

Guidance literature:: With potassium carbonate; In water; acetone; for 2.5h; Heating;
DOI:10.1016/S0223-5234(99)80082-8

Reference yield:

: 536-90-3,918666-97-4
m-Anisidine

: 247031-67-0
N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: 80 percent / tetrahydrofuran / 20 h / Heating

2: 62 percent / K₂CO₃ / acetone; H₂O / 2.5 h / Heating

With potassium carbonate; In tetrahydrofuran; water; acetone; 1: Substitution / 2: Cyclization;
DOI:10.1016/S0223-5234(99)80082-8

Reference yield:

: C₈H₇NO₂S₃^(2-)*2Na⁽¹⁺⁾

: 247031-67-0
N-[4-hydroxy-3-(3-methoxyphenyl)-2-thiazolidinylidene]-4-methylphenylsulfonamide

Guidance literature:: Multi-step reaction with 3 steps

1: dimethylformamide / 2 h / 20 °C

2: 80 percent / tetrahydrofuran / 20 h / Heating

3: 62 percent / K₂CO₃ / acetone; H₂O / 2.5 h / Heating

With potassium carbonate; In tetrahydrofuran; water; N,N-dimethyl-formamide; acetone; 1: Methylation / 2: Substitution / 3: Cyclization;
DOI:10.1016/S0223-5234(99)80082-8