4-ferrocenyl-2-nitrophenol

Base Information

Chemical Name:4-ferrocenyl-2-nitrophenol
CAS No.:868762-22-5
Molecular Formula:C₁₆H₁₃FeNO₃
Molecular Weight:323.131
Hs Code.:

Synonyms:4-ferrocenyl-2-nitrophenol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-ferrocenyl-2-nitrophenol

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Technology Process of 4-ferrocenyl-2-nitrophenol

There total 1 articles about 4-ferrocenyl-2-nitrophenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 36.0%

: 102-54-5,55404-68-7
ferrocene

: 119-34-6
4-amino-2-nitrophenol

: 868762-22-5
4-ferrocenyl-2-nitrophenol

Guidance literature:: With H₂SO₄; NaNO₂; HCl; copper; In water; ferrocene added to H2SO4, stirred at room temp., poured into H2O (ice bath); aq. soln. of NaNO2 added dropwise to a soln. of 2-nitro-4-aminophenol in aq. HCl at 0°C, stirred, added to the soln. of Fe complex at 0°C,; Cu powder added, allowed to warm to room temp., stirred, ascorbic acid added, CH2Cl2 added, filtered, the org. layer sepd., the aq. layer extd. (CH2Cl2), the org. exts. dried, filtered, solvent-removed, chromd., solvent-removed, recrystd.;
DOI:10.1021/ic051184r

Reference yield: 74.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 868762-22-5
4-ferrocenyl-2-nitrophenol

: 868761-99-3
2-amino-4-ferrocenylphenol hydrochloride

Guidance literature:: With Sn; In hydrogenchloride; ethanol; refluxed for 1 h; cooled, filtered, washed (cold MeOH, CHCl3);
DOI:10.1021/ic051184r