(+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile

Base Information

Chemical Name:(+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile
CAS No.:110654-71-2
Molecular Formula:C₂₁H₂₉NOS₂
Molecular Weight:375.599
Hs Code.:

Synonyms:(+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile

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Chemical Property of (+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile

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Technology Process of (+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile

There total 3 articles about (+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 90122-60-4,92830-58-5,92830-59-6,110654-69-8
(+/-)-(1RS,2SR)-2-<2-(2-methoxyphenyl)-ethyl>-1,3,3-trimethyl-5-oxocyclohexanecarbonitrile

: 540-63-6
ethane-1,2-dithiol

: 110654-71-2
(+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile

Guidance literature:: With boron trifluoride diethyl etherate; In dichloromethane; for 5h; Ambient temperature;

Reference yield:

: 90122-59-1
4-<2-(2-methoxyphenyl)ethyl>-3,5,5-trimethylcyclohex-2-enone

: 110654-71-2
(+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / triethylaluminium / tetrahydrofuran / 22 h / Ambient temperature

2: 92 percent / boron trifluoride-diethyl ether / CH₂Cl₂ / 5 h / Ambient temperature

With boron trifluoride diethyl etherate; triethylaluminum; In tetrahydrofuran; dichloromethane;

Reference yield:

: 31225-15-7
2-methoxybenzylmagnesium bromide

: 110654-71-2
(+/-)-(1RS,2SR)-5,5-ethylenedithio-2-<2-(2-methoxyphenyl)ethyl>-1,3,3-trimethylcyclohexanecarbonitrile

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) copper(I)bromide; 2.) aq. HCl / 1.) diethyl ether, THF, 0 deg C; rt, 0.5 h; 2.)THF, reflux, 2 h.

2: 71 percent / triethylaluminium / tetrahydrofuran / 22 h / Ambient temperature

3: 92 percent / boron trifluoride-diethyl ether / CH₂Cl₂ / 5 h / Ambient temperature

With hydrogenchloride; boron trifluoride diethyl etherate; triethylaluminum; copper(I) bromide; In tetrahydrofuran; dichloromethane;