N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide

Base Information

• Chemical Name: N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide
• CAS No.: 1407510-85-3
• Molecular Formula: C₈₁H₇₉N₇O₁₉
• Molecular Weight: 1454.55

Synonyms:N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide

Chemical Property of N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide

Chemical Property:

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Technology Process of N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide

There total 1 articles about N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

3,4-bis(benzyloxy)-5-(((3S,7S,11S)-7,11-bis(2,3-bis-(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)carbamoyl)benzoic acid (1407510-70-6) + 2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethylamine (134179-38-7) → N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N3-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide (1407510-85-3)

Guidance literature:

With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 4h;

DOI:10.1021/ja3077268

Reference yield: 28.0%

N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N3-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide (1407510-85-3) → N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N3-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide (1616700-71-0)

Guidance literature:

N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N₃-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide; With pentamethylbenzene,; boron trichloride; In dichloromethane; at -78 ℃; for 1.5h; Inert atmosphere;

With methanol; N-ethyl-N,N-diisopropylamine; In dichloromethane; at -78 - 20 ℃; Inert atmosphere;

DOI:10.1021/ja503911p

Reference yield:

N1-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-4,5-bis(benzyloxy)-N3-((3S,7S,11S)-7,11-bis(2,3-bis(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)isophthalamide (1407510-85-3) → C76H81N9O24S

Guidance literature:

With copper(II) sulfate; sodium L-ascorbate; tris[(1-benzyl-1H-1,2,3-triazol-4yl)methyl]amine; In water; dimethyl sulfoxide; at 20 ℃;

upstream raw materials:

3,4-bis(benzyloxy)-5-(((3S,7S,11S)-7,11-bis(2,3-bis-(benzyloxy)benzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)carbamoyl)benzoic acid

2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethylamine

Downstream raw materials:

tert-butyl(2-(((1-(1-(3-(((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)carbamoyl)-4,5-dihydroxyphenyl)-1-oxo-5,8,11-trioxa-2-azatridecan-13-yl)-1H-1,2,3-triazol-4-yl)methyl)amino)-2-oxoethyl)carbamate

N₁-(2-(2-(2-(2-azidoethoxy)ethoxy)ethoxy)ethyl)-N₃-((3S,7S,11S)-7,11-bis(2,3-dihydroxybenzamido)-2,6,10-trioxo-1,5,9-trioxacyclododecan-3-yl)-4,5-dihydroxyisophthalamide

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