rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol

Base Information

• Chemical Name: rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol
• CAS No.: 756531-64-3
• Molecular Formula: C₆₃H₈₀Cl₂N₂O₈
• Molecular Weight: 1064.24

Synonyms:rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol

Chemical Property of rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol

Chemical Property:

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Technology Process of rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol

There total 3 articles about rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-Boc-merphalan + rac-1-(Z-9-octadeceyl)-3-[3-(3-perylenoyl)propionyl]glycerol (756531-63-2) → rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol (756531-64-3)

Guidance literature:

With dmap; dicyclohexyl-carbodiimide; In tetrachloromethane; chloroform; for 24h;

DOI:10.1023/B:RUBI.0000015776.60923.96

Reference yield:

rac-1-(Z-9-octadecenyl)glycerol (593-31-7) → rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol (756531-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / DCC; 4-dimethylaminopyridine / CHCl₃; CCl₄ / 24 h

2: 70 percent / DCC; 4-dimethylaminopyridine / CHCl₃; CCl₄ / 24 h

With dmap; dicyclohexyl-carbodiimide; In tetrachloromethane; chloroform;

DOI:10.1023/B:RUBI.0000015776.60923.96

Reference yield:

3-(3-perylenoyl)propionic acid (110774-35-1) → rac-1-(Z-9-octadecenoyl)-2-(N-Boc-merphalanyl)-3-[3-(3-perylenoyl)propionyl]glycerol (756531-64-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 45 percent / DCC; 4-dimethylaminopyridine / CHCl₃; CCl₄ / 24 h

2: 70 percent / DCC; 4-dimethylaminopyridine / CHCl₃; CCl₄ / 24 h

With dmap; dicyclohexyl-carbodiimide; In tetrachloromethane; chloroform;

DOI:10.1023/B:RUBI.0000015776.60923.96

upstream raw materials:

rac-1-(Z-9-octadeceyl)-3-[3-(3-perylenoyl)propionyl]glycerol

rac-1-(Z-9-octadecenyl)glycerol

3-(3-perylenoyl)propionic acid

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