C₂₈H₃₉NO₅Si

Base Information

Chemical Name:C₂₈H₃₉NO₅Si
CAS No.:1262959-05-6
Molecular Formula:C₂₈H₃₉NO₅Si
Molecular Weight:497.707
Hs Code.:

C<sub>28</sub>H<sub>39</sub>NO<sub>5</sub>Si

Synonyms:C₂₈H₃₉NO₅Si

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Chemical Property of C₂₈H₃₉NO₅Si

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Technology Process of C₂₈H₃₉NO₅Si

There total 1 articles about C₂₈H₃₉NO₅Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1262959-01-2
C₂₂H₂₅NO₄

: 76513-69-4
(2-trimethylethylsilylethoxy)methyl chloride

: 1262959-05-6
C₂₈H₃₉NO₅Si

Guidance literature:: C₂₂H₂₅NO₄; With potassium hexamethylsilazane; In tetrahydrofuran; toluene; at -78 ℃; for 0.5h; Inert atmosphere;

(2-trimethylethylsilylethoxy)methyl chloride; In tetrahydrofuran; toluene; at -78 - 20 ℃; for 2.75h; Inert atmosphere;
DOI:10.1021/jo1019927

Reference yield: 70.0%

: 1262959-05-6
C₂₈H₃₉NO₅Si

: 1262959-04-5
C₂₃H₂₇NO₅

Guidance literature:: C₂₈H₃₉NO₅Si; With boron trifluoride diethyl etherate; In toluene; at 0 - 20 ℃; for 20h; Inert atmosphere;

With water; sodium hydrogencarbonate; In toluene;
DOI:10.1021/jo1019927

Reference yield:

: 1262959-05-6
C₂₈H₃₉NO₅Si

: 1262959-03-4
C₂₃H₂₅NO₅

Guidance literature:: Multi-step reaction with 2 steps

1: boron trifluoride diethyl etherate / toluene / 20 h / 0 - 20 °C / Inert atmosphere

2: oxalyl dichloride; dimethyl sulfoxide; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

With oxalyl dichloride; boron trifluoride diethyl etherate; dimethyl sulfoxide; triethylamine; In dichloromethane; toluene; 2: Swern oxidation;
DOI:10.1021/jo1019927